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Korean Journal of Dental Materials

1966  (1,  1)  to  Present  ISSN: 2384-4434

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Effects of thermoplastic appliance fabrication on the dimensional stability of 3D printed dental models

Byung-Min KANG ; Sung-Kwon CHOI

Korean Journal of Dental Materials.2020;47(2):105-118. doi:10.14815/kjdm.2020.47.2.105

The purpose of this study was to evaluate effects of fabrication of thermoplastic appliance on the dimensional stability of 3D printed dental models. A digital reference model was printed by different printing materials and densities [acrylonitrile butadiene styrene (ABS) and polylactic acid (PLA); 20, 40 and 60%]. Thermoplastic appliances were then fabricated with printed models for three times and models were scanned at three different stated; following the print out, following the fabrication for one time and three times. Tooth and arch measurements were performed to evaluate the accuracy and dimensional stability of printed models after fabrication of thermoplastic appliances. Printed models were not significantly different from the digital reference model regardless of different materials and densities. After the first fabrication of the appliance, most of measurements were decreased in PLA models ranged from 0.05 to 0.24 mm (p<0.05), whereas only a few measurements were decreased in ABS models (p<0.05). After fabrication for three times, measurements were more decreased in PLA models ranged from 0.04 to 0.42 mm (p<0.05) and some measurements were decreased in ABS models ranged from 0.08 to 0.27 mm (p<0.05). ABS models showed relatively good dimensional stability, but the PLA models showed significant dimensional changes even after initial fabrication of the appliance. Repeated fabrication of the appliances increased dimensional changes in printed models, especially printed with PLA.

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Diffuse reflection characterization and visible light mediated antibacterial effect of Pt-TiO2 nanotubes

Kyung-Suk MOON ; Ji-Myung BAE ; Seunghan OH

Korean Journal of Dental Materials.2020;47(2):93-104. doi:10.14815/kjdm.2020.47.2.93

The purpose of this study was to fabricate platinum (Pt), one of the plasmonic nanoparticles that induces localized surface plasmon resonance (LSPR) effects caused by the pairing of plasmon with the electric field of visible-near infrared light, coated 100 nm titania (Pt-TiO2) nanotubes to evaluate the surface properties and laser mediated antibacterial effects. From the analysis of UV-VIS-NIR spectrum, the light absorptions of Pt-TiO2 nanotubes were detected at wavelengths 399–429 nm, 527–579 nm, and 806–906 nm, respectively, and one of the detected wavelengths was suitable for the laser used in this study (OCLA, Wavelength: 405). From the observation of FE-SEM, as the platinum coating time increased, the inner diameter of the Pt-TiO2 nanotubes decreased from 68.8 nm to 48.8 nm, and the shape of the platinum nanoparticles coated on the top layer of the titania nanotubes changed from spherical to rod. From the results of contact angle measurement, the contact angle of water increased from 11.94°to 19.84°as the platinum coating time increased from 1 minute to 3 minutes. The Staphylococcus aureus antibacterial test resulted that 98% or more bacterial reduction of all Pt-TiO2 nanotube groups were observed after laser irradiation (P<0.05). Live-dead assay and MTT assay indicated that laser irradiation did not affect cell death. Therefore, Pt–TiO2 nanotube exhibiting a local surface plasmon resonance effect is expected to have many potentials for semi-permanent antimicrobial implant surface treatment without antibacterial drugs.

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Shear bond strength between orthodontic metal brackets and Y-TZP according to the various ceramic surface treatments before and after thermocycling

Ji-Bong CHOI ; Seon-Mi BYEON

Korean Journal of Dental Materials.2020;47(2):83-92. doi:10.14815/kjdm.2020.47.2.83

In this study, clinically applicable methods of improving the bond strength between Y-TZP and the bracket were considered, which the method was confirmed for the durability in a humid oral environment. The bond strength of Y-TZP bonding surface and the surface characteristics were analyzed following the surface treatment of Y-TZP specimens with conditioning by 30 μm tribochemical silica coating, or tribochemical silica coating with one of the following primers: silane, MDP, or an MDP-containing silane primer. It was found that after surface treatment, the surface roughness of all groups increased (p<0.05), and Si was uniformly distributed on the Y-TZP surface after silica coating. The bond strength value of the group treated with silane primer and tribochemical coating was not significantly different after thermocycling (p>0.05). The group treated with MDP primer and tribochemical silica coating showed a significant difference in bond strength values after thermocycling (p<0.05), and it showed the lowest bond strength values except the untreated groups (p<0.05). The group treated with tribochemical silica coating and MDP-containing silane primer showed the highest bond strength values (p<0.05), and was not significantly different after thermocycling (p>0.05). Therefore, the surface treatments of Y-TZP with MDP-containing silane primer after 30 μm tribochemical silica coating enhanced the bond strength to the orthodontic metal bracket; such a clinically applicable method may advance studies on the surface treatment of Y-TZP.

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Antibacterial activity and characterization of tissue conditioner containing silver-chitosan nanocomplex

Ki Young NAM

Korean Journal of Dental Materials.2020;47(2):71-82. doi:10.14815/kjdm.2020.47.2.71

The objective of this work was to verify the antimicrobial effect and the characteristics of the tissue conditioner containing silver-chitosan nanocomplex at in vitro level. Nanocomplex was synthesized by the chemical reduction of silver nitrate and chitosan in aqueous solution with sodium borohydride as a reducing agent. Silver-chitosan nanocomplex was incorporated to tissue conditioner as powder to powder ratio with different weight percentage (%) of 0 (control), 1.0, 3.0, 5.0 and 7.0. The antimicrobial effect was assessed by colony forming unit in retrieved two streptococcal suspensions inoculated on specimens and cytotoxicity was measured using human gingival fibroblasts by MTS assay. Surface topography, Ag ion release and ultimate tensile strength tests were conducted for mechanical validity. The significantly reduced bacterial adhesions were observed above 5.0% loading while all of tested samples did not show cytotoxicity when compared to the control. Ag ion releases were detected with the dose-dependent of initial silver loadings with gradual decreasing over time. Modified tissue conditioner revealed similar microscopic surface textures and expressed no significant tensile strength changes (P>0.01) as compared to unmodified. Within some limitations in present study, the tissue conditioner loaded by 5.0% of silver-chitosan nanocomplex can be candidate as a novel denture biomaterial without mechanical hazards. For a clinical specification, future studies including in vivo, multi-strain or factor assays, and additional physical tests were still required.

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Sustainability of the antibacterial activity of experimental fluoride varnish mixed with antibacterial agents against Streptococcus mutans

Ju-Lee SON ; Ji-Myung BAE

Korean Journal of Dental Materials.2020;47(2):63-70. doi:10.14815/kjdm.2020.47.2.63

This study aimed to assess the sustainability of antibacterial agents mixed with experimental fluoride varnish (EFV) against S. mutans. Five antibacterial agents [Xanthorrhizol (XAN), Bakuchiol (BAK), Bavachalcone (BCC), Isobavachromene (IBC), and Bavachromene (BCM)] were used and incorporated into the EFV to make the final concentration of 10 mM. Then, 5 μL of antibacterial agents mixed with EFV were applied on polyethylene terephthalate film disc (5 mm diameter). The positive and vehicle control were ampicillin and DMSO mixed with EFV, respectively. Each group was stored in distilled water in a 37℃ shaking water bath at 80 rpm for 0 hour, 4 hours, 1 day, 2 days, 3 days, 5 days, 10 days, 20 days and 30 days. The sustainability of the antibacterial activities was evaluated with the inhibition zone by the agar diffusion test. The antibacterial activities of all antibacterial agents were sustained for 30 days. Among them, BCC showed relatively higher antibacterial activities up to 30 days compared to other groups. This study suggests that antibacterial agents including BCC can be used with fluoride varnish to have sustained antibacterial activities.

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Osteoblast cytocompatibility and antibacterial effect of ginger main compounds

Regina Guadalupe ARBIZÚ-TRIGUEROS ; Young-Seon BAEK ; Seo-Young KIM ; Yu-Kyoung KIM ; Yong-Seok JANG ; Tae-Hwan KIM ; Tae-Sung BAE ; Min-Ho LEE

Korean Journal of Dental Materials.2021;48(3):159-174. doi:10.14815/kjdm.2021.48.3.159

Ginger has been used worldwide in traditional medicine. It has been reported that phenolic compounds such as gingerol and shogaol in ginger have beneficial cellular effect and antibacterial effect. The purpose of this study was to investigate the effect of gingerol and shogaol on the cytocompatibility for the osteoblastic cells and antibacterial activity against oral microorganisms. Chemical structures of gingerol and shogaol were determined by Fourier transform infrared (FT-IR). Thermal and pH stability was analyzed by UPLC assay. Streptococcus mutans, and Porphyromonas gingivalis were used to confirm the antibacterial effect of the ginger compounds and MC3T3-E1 cells were used to identify biocompatibility test. Cell viability and bacterial growth was determined by water-soluble tetrazolium salt (WST-8) colorimetric assay. Cellular morphology was identified with optical microscope after crystal violet staining. Cell differentiation and oxidative stress were evaluated by Alkaline phosphatase (ALP) assay and hydrogen peroxide colorimetric assay. The chemical bonding related with hydroxyl groups, carbonyl groups and aromatic ring was identified in all ginger compounds. Gingerol and shogaol presented good stability at acid and neutral pH at room temperature. All compounds showed better antibacterial effect against Porphyromonas gingivalis than Streptococcus mutans. 10-gingerol and all shogaol groups below 10-6 M presented suitable cytocompatibility for osteoblastic cells compared to control group. All groups showed similar Oxidative stress to control group, and ALP activity in all groups below 10-6 M was not statistically significant compared to control. Hence, this study concludes that shogaol groups presented better antibacterial effect and suitable cytocompatibility than gingerol groups.

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Color stability of esthetic restorative materials after application of fluoride varnishes

Chul-Hoon JANG ; Dong-Gil JANG ; Bin-Na LEE ; Hoon-Sang CHANG ; Yun-Chan HWANG ; Won-Mann OH ; In-Nam HWANG

Korean Journal of Dental Materials.2021;48(3):147-158. doi:10.14815/kjdm.2021.48.3.147

The objective of present study was to compare the color stability of esthetic materials after application of fluoride varnishes. Esthetic restorative materials including composite resin (Filtek Z350 XT, 3M ESPE, MN, USA), resin modified glass-ionomer (RMGI, Fuji II LC, GC Co., Tokyo, Japan), and giomer (Beautifil Flow Plus F00, Shofu Inc., Kyoto, Japan) were used in this study. Cavity shield (3M ESPE, MN, USA) and V-varnish premium (Vericom, Seoul, Korea) were used as the fluoride varnishes. 30 samples of each restorative materials were prepared, which were divided into 10 each, among three groups. Group I were stored in distilled water, which were used as the control, Group II were applied with Cavity shield and Group III were applied with V-varnish premium. All specimens were stored in the distilled water at 60 ℃ for 30 days for the accelerated test. Samples were then subjected to colorimetric analysis. Data collected was statistically analyzed using one way ANOVA and Tukey's post-hoc test (p=0.05). The color change before and after application of varnish was observed in all experimental groups. Especially RMGI showed highest ΔE* value (p<0.05). The color change according to the accelerated test showed no significant difference in the varnish application group and the control group. Giomer and RMGI applied with Cavity shield showed more color change than V-varnish applied group, despite no significant differences. Present study concludes that color stability of esthetic restoration materials can be affected by application of fluoride varnish. Especially, RMGI showed a large color change compared to the composite resin and giomer, which suggested that careful attention should be paid to clinical application.

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The effect of agitation and evaporating time of a newly released universal adhesive on dentin bond strength

Soo-Min AHN ; Jeong-Kil PARK ; Sung-Ae SON

Korean Journal of Dental Materials.2021;48(3):135-146. doi:10.14815/kjdm.2021.48.3.135

Universal adhesives that simplify bonding procedures and be used in multi-etch mode have been developed. In this study, the effects of agitation and solvent evaporation time of a universal adhesive on microtensile bond strength (µTBS) were evaluated by varying the times of these two procedures. Eighteen human molars were used to fabricate specimens, and the teeth were randomly divided into six experimental groups. Each group had different agitation time (5 s, 10 s, 20 s) and evaporation time (10 s, 20 s). The specimens were cut into a rod-shape with a cross-sectional area of 1 mm2 , and their µTBS was measured. The data were analyzed using an ANOVA and Tukey’s post hoc test. After this, the debonded surface was observed using scanning electron microscopy (SEM). In the groups with a solvent evaporation time of 20 s, µTBS was statistically higher, even with a short agitation time (p<0.05). Furthermore, for the groups with the shorter evaporation time, bonding strength decreased statistically as the agitation time shortened (p<0.05). The results of this experiment suggest that if the solvent was adequately evaporated, sufficient bonding strength could be obtained even when the adhesive was agitated for a short time. This is supported by the results of SEM image analysis, which revealed a uniform adhesive layer with well-infiltrated tags in the groups with the prolonged evaporation time. It may be crucial to secure an adequate evaporation time in order to obtain optimal bonding strength.

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Evaluation of bioactivity and osseointegration for ti-6al-4v alloy implant modified by anodic oxidation and cyclic precalcification treatments

Yong Seok JANG ; Jae Yoen KANG ; Kang Gyu LEE ; Chung Ha LIM ; Min Ho LEE ; Tae Sung BAE

Korean Journal of Dental Materials.2019;46(1):43-52. doi:10.14815/kjdm.2019.46.1.43

The aim of this study was to examine the bioactivity and osseointegration of Ti-6Al-4V alloy implant which was modified by an anodic oxidation and a cyclic precalcification treatments. After blasting treatment using HAp (Hydroxyapatitie; HAp) powder which is resorbable blasting media (RBM) on the surface of Ti-6Al-4V alloy implants, the anodic oxidation treatment and the cyclic precalcification treatment were conducted to form nanotube TiO2 layer and HAp precipitation respectively. The surface morphology of the surface-treated Ti-6Al-4V alloy implant was investigated after immersion in the simulated body fluid(SBF) for 3 days to investigate the bioactivity. To investigate the effect of surface treatment on bonding between the implant and bone, RBM treated implant and RBM-anodization-cyclic precalcification(RACP) treated implant were placed on the distal side of both tibia diaphysis of rats, and then the removal torque of the implant was measured after 4 weeks. On the surface of RACP treated group, bone-like apatite precipitation was observed after immersion in SBF for 3 days. The removal torque was significantly higher in the RACP treated group than in the RBM treated group. The interfacial fracture between the implant and the new bone was observed in the RBM treated group, but both the cohesive fracture at the new bone and the interfacial fractures between the implant and the new bone were observed in the RACP treated group.
Alloys ; Animals ; Diaphyses ; Immersion ; Nanotubes ; Osseointegration ; Rats ; Tibia ; Torque

Alloys ; Animals ; Diaphyses ; Immersion ; Nanotubes ; Osseointegration ; Rats ; Tibia ; Torque

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Surface characterization of calcium phosphate coating formed on chitosan and alkali-treaDted titanium metal

Kyung Hee PARK ; Woon Young LEE ; Ho Ju SONG ; Yeong Joon PARK

Korean Journal of Dental Materials.2019;46(1):33-42. doi:10.14815/kjdm.2019.46.1.33

The calcium phosphate coating on various pretreated metals was prepared by soaking in modified simulated body fluid (m-SBF) solution. The coating structure and its surface morphologies were determined by x-ray diffraction, Fourier transform infrared spectroscopy, and scanning electron microscopy. The results revealed significant differences in morphology and composition of the calcium phosphate coatings with and without chitosan and NaOH-pretreated commercially pure titanium (cp-Ti) substrate. The calcium phosphates formed on chitosan coated-Ti pretreated with NaOH were ~ 350 nm-sized resulting in strong bonding of the apatite layer with the substrates and a uniform gradient of stress transfer from coating materials to the Ti-substrate. After NaOH pretreatment, the hydroxyl groups bind to Ca²⁺ to attract PO₄³⁻ anions, eventually resulting in a continuous layer of calcium phosphate on chitosan coated-Ti substrate during immersion in m-SBF solution. The chitosan coated-Ti showed hydrophobic surface while NaOH pretreatment resulted in maximum hydrophilicity to the Ti substrate. Due to improved wettability of Ti by NaOH pretreatment before chitosan coating, aggregation of calcium phosphate was prevented and size-controlled composite materials were obtained.
Anions ; Body Fluids ; Calcium Phosphates ; Calcium ; Chitosan ; Clothing ; Hydrophobic and Hydrophilic Interactions ; Immersion ; Metals ; Microscopy, Electron, Scanning ; Spectroscopy, Fourier Transform Infrared ; Titanium ; Wettability ; X-Ray Diffraction

Anions ; Body Fluids ; Calcium Phosphates ; Calcium ; Chitosan ; Clothing ; Hydrophobic and Hydrophilic Interactions ; Immersion ; Metals ; Microscopy, Electron, Scanning ; Spectroscopy, Fourier Transform Infrared ; Titanium ; Wettability ; X-Ray Diffraction

Country

Republic of Korea

Publisher

Korean Society for Dental Materials

ElectronicLinks

http://www.kadm.org

Editor-in-chief

Seunghan Oh

E-mail

ksdmwku@gmail.com

Abbreviation

Korean J Dent Mater

Vernacular Journal Title

대한치과재료학회지

ISSN

2384-4434

EISSN

2384-3268

Year Approved

2018

Current Indexing Status

Currently Indexed

Start Year

1966

Description

Korean Journal of Dental Materials is the official journal of Korean Society for Dental Materials. The journal provides rapid publication high-quality dental research in the areas of dental materials and their clinical applications since 1966.

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