Determination of sabinene in ledum terpenes from Ledum palustry L by gas chromatography
- VernacularTitle:气相色谱法测定杜香萜烯中的桧烯含量
- Author:
Fengrong ZHANG
;
Yanbin SU
;
Zhenling LIU
;
Yanwen SU
;
Zhuosong JANG
;
- Publication Type:Journal Article
- Keywords:
sabinene;
ledum terpenes;
Ledum palustry L;
gas chromatography
- From:
Chinese Traditional Patent Medicine
1992;0(05):-
- CountryChina
- Language:Chinese
-
Abstract:
AIM: To establish a gas chromatography method for the determination of sabinene in ledum terpenes from Ledum palustry L. METHODS: 5% SE 30 was adopted as the stationary phase, the temperature of column was set at 65 ?C and FID detector with termperature at 200 ?C . RESULTS: Sabinene in the preparation was gained satisfactory separation and assay under the chromatographic condition. The calibration curve of sabinene was good linear in the range of 0.06 0.60 mg?mL -1 . with the corelation coefficient r=0.9998(n=6) . The average recovery of sabinene was 100.3%, RSD=1.4%, (n=5) . CONCLUSION: The method is simple, highly repeatable and accurate, and it can be used to control the quality of the preparation.
