HPLC fingerprint of Fritillaria hupehensis.
- Author:
Guo-Xin ZHANG
1
;
Juan LI
;
Peng ZHANG
;
Han-Li RUAN
;
Yong-Hui ZHANG
;
Hui-Fang PI
;
Ji-Zhou WU
Author Information
- Publication Type:Journal Article
- MeSH: Alkaloids; analysis; Cevanes; analysis; Chromatography, High Pressure Liquid; methods; Fritillaria; chemistry; Light; Plant Roots; chemistry; Plants, Medicinal; chemistry; Quality Control; Reproducibility of Results; Scattering, Radiation; Sensitivity and Specificity
- From: Acta Pharmaceutica Sinica 2005;40(9):850-853
- CountryChina
- Language:Chinese
-
Abstract:
AIMTo establish a fingerprint analysis method of Fritillaria hupehensis.
METHODSfingerprint was performed by HPLC-ELSD. Hypersil ODS column was used; the mobile phase was composed of methanol (with 0.05% triethylamine) and water with gradient elution; flow rate was 1.0 mL x min(-1); recording time was 60 min; drift tube temperature was 75 degrees C; gas flow rate was 1.9 L x min(-1).
RESULTSHPLC fingerprint of Fritillaria hupehensis was obtained.
CONCLUSIONA reliable method was provided for controlling the quality of Fritillaria hupehensis.
