1.HPLC-ELSD for determining contents of three triterpenoidal saponins in fruits of Buddleja lindleyana from different habitats.
Pei-Yun WU ; Ya-Shuo REN ; De-Ling WU ; Jin-Wei QIAO
China Journal of Chinese Materia Medica 2016;41(7):1218-1221
To establish an HPLC-ELSD method for the quantification of triterpenoids in the fruits of Buddleja lindleyana. The RP-HPLC-ELSD method was used for the determination of triterpenoids in B. lindleyana fruits, which were collected from different habitats. The column used was a packed with 5 μm stationary phase Waters SunFireTM C₁₈ (4.6 mm×150 mm, 5 μm). The mobile phase consisted of Methanol-water(82∶18) at a flow rate of 1 mL•min⁻¹. Column temperature: 30 ℃. ELSD conditions: drift tube temperature: 106 ℃; carrier gas (nitrogen) flow rate: 1.5 L•min⁻¹; amplification factor: 1. The calibration curves showed good linear relationship on a range from 0.702 to 28.08 μg(r=0.999 2) for Clinoposaponin III, 0.390 to 15.60 μg(r=0.998 9) for Desrhamnoverbascosaponin and 0.192 to 7.68μg(r=0.999 0) for Mimengoside I. The average recovery rate(n=6) were 99.41%, 99.08% and 98.67% and it's RSD were 0.86%, 1.56% and 1.80%. This method can be used to determine the contents of triterpenoids in the fruits of Buddleja lindleyana for its simplicity, accurateness and reliability.
2.Fluorodeoxyglucose positron emission tomography/computed tomography and magnetic resonance imaging of uterine leiomyosarcomas: 2 cases report.
Hui-juan ZHANG ; Feng-hua ZHAN ; Ya-jun LI ; Hao-ran SUN ; Ren-ju BAI ; Shuo GAO
Chinese Medical Journal 2011;124(14):2237-2240
Uterine leiomyosarcoma is an uncommon malignant neoplasm of smooth muscle origination and is associated with a poor prognosis. We report two cases of uterine leiomyosarcoma that presented with pulmonary metastases. 2-deoxy-2-(¹⁸F)fluorodeoxyglucose (FDG) positron emission tomography (PET)/computed tomography (CT) was performed to identify the primary carcinoma and found the focus located in the uterus. The follow-up magnetic resonance imaging (MRI) confirmed the diagnosis was uterine leiomyosarcoma.
Adult
;
Female
;
Fluorodeoxyglucose F18
;
Humans
;
Leiomyosarcoma
;
diagnosis
;
Magnetic Resonance Imaging
;
methods
;
Middle Aged
;
Positron-Emission Tomography
;
methods
;
Tomography, X-Ray Computed
;
methods
;
Uterine Neoplasms
;
diagnosis
3.Imaging features of primary adrenal lymphoma.
Jun-ping WANG ; Hao-ran SUN ; Ya-jun LI ; Ren-ju BAI ; Shuo GAO
Chinese Medical Journal 2009;122(20):2516-2520

Result Analysis
Print
Save
E-mail