A new diterpenoid acid from the rosin of Pinus kesiya var. langbianensis (A.Chev.) Gaussen ex Bui
10.16438/j.0513-4870.2022-0432
- VernacularTitle:思茅松松脂中一个新的二萜酸
- Author:
Yu-fei LIU
1
;
Yan-zhi WANG
2
;
Zhi-min SONG
1
;
Lin-qing QIAO
1
;
Rui PENG
1
;
Wei-sheng FENG
2
;
Yong-xian CHENG
3
Author Information
1. School of Pharmacy, Henan University of Chinese Medicine, Zhengzhou 450046, China
2. School of Pharmacy, Henan University of Chinese Medicine, Zhengzhou 450046, China; Collaborative Innovation Center for Chinese Medicine and Respiratory Diseases Co-constructed by Henan Province & Education Ministry of P.R. China, Zhengzhou 450046, China
3. School of Pharmaceutical Sciences, Institute for Inheritance-Based Innovation of Chinese Medicine, Shenzhen University, Shenzhen 518060, China
- Publication Type:Research Article
- Keywords:
italic>Pinus kesiya var. langbianensis (A.Chev.) Gaussen ex Bui;
rosin;
iterpenoid acid;
extraction and separation;
chemical composition
- From:
Acta Pharmaceutica Sinica
2022;57(9):2786-2790
- CountryChina
- Language:Chinese
-
Abstract:
One undescribed diterpenoid acid and six compounds were isolated from the 95% ethanol fraction of Pinus kesiya var. langbianensis (A.Chev.) Gaussen ex Bui resin by using various chromatographic methods, including MCI Gel, Sephadex LH-20, ODS, silica gel and semi-preparative HPLC. The planar structures were identified by spectroscopy methods (1D, 2D NMR, UV, IR, MS, etc.), and the absolute configuration of the new compound was determined by ECD calculation. Compound 1 is a new compound, and compounds 2, 5-7 were isolated from Pinus kesiya var. langbianensis (A.Chev.) Gaussen ex Bui for the first time.