Chemical constituents from the petroleum ether fraction of the roots of Gypsophila licentiana
10.3969/j.issn.1001-1528.2025.03.018
- VernacularTitle:细叶石头花根石油醚部位化学成分研究
- Author:
Zhi-ning GAO
1
;
Tian-tian QIU
;
Tian-yi CUI
;
Xiao-ya SUN
;
Shu-juan XUE
;
Sui-qing CHEN
Author Information
1. 河南中医药大学药学院,河南郑州 450046
- Publication Type:Journal Article
- Keywords:
Gypsophila licentiana Hand.-Mazz.;
roots;
Gypsophilae Radix;
petroleum ether fraction;
chemical constituents;
isolation and identification
- From:
Chinese Traditional Patent Medicine
2025;47(3):821-827
- CountryChina
- Language:Chinese
-
Abstract:
AIM To study the chemical constituents from the petroleum ether fraction of the roots of Gypsophila licentiana Hand.-Mazz.METHODS Silica gel,Sephadex LH-20 and semi-preparative HPLC were used for isolation and purification,then the structures of obtained compounds were identified by physicochemical properties and spectral data.RESULTS Eighteen compounds were isolated and identified as dibutyl phthalate(1),glyceryl arachidate(2),bis(2-ethylhexyl)terephthalate(3),9,12-octadecadienoic acid(Z,Z)-methyl ester(4),(3'S,4'S)-3'-acetoxy-4'-angeloyloxy-3',4'-dihydroseselin(5),3-(4-hydroxy-3-methoxyphenyl)-propanoic acid(6),bis(2-ethylhexyl)phthalate(7),2,2'-oxybis(1,4)-di-tert-butylbenzene(8),gypsogenin(9),3-keto,16α-hydroxy,24-noroleanolic acid(10),3-oxo-olean-12-en-28-oic acid(11),10-eicosenoic acid(12),hexacosanic acid(13),enniatin B(14),(R,Z)-21-methyl-8-pentatriacontene(15),ethyl gallate(16),stellarine A(17),pentacosane(18).CONCLUSION All compounds are isolated from this plant for the first time.
