1.Chemical constituents in root of Hemerocallis fulva.
Zhong-Duo L YANG ; Tao LI ; Yuan-Chao LI
China Journal of Chinese Materia Medica 2008;33(3):269-272
OBJECTIVETo study the chemical constituents of the root of Hemerocallis fulva.
METHODCompounds were isolated by repeated silica gel, Sephadex LH-20, MCI gel, etc. column chromatography and their structures were determined by spectral analyses and physicochemical properties.
RESULTFrom the n-butanol fraction of the EtOH extract of the roots of H. fulva, 9 glycosides were isolated and identified as sweroside (1), laganin (2), picraquassioside C (3), puerarin (4), 3'-methoxypuerarin (5), 7-hydro xylnaphthalide-O-beta-D-glucopyranoside (6), orcinol-3-O-beta-glucopyranoside (7), HN saponin F (8), hederagenin-3-0-beta D-glucopyranosyl-(1-3)-alpha-L-arabinopyranoside-28-O-beta-D-glucopyranosyl ester (9).
CONCLUSIONCompounds 1-9 were isolated from the genus Hemerocallis for the first time.
Glucosides ; chemistry ; isolation & purification ; Hemerocallis ; chemistry ; Iridoid Glucosides ; Iridoids ; chemistry ; isolation & purification ; Isoflavones ; chemistry ; isolation & purification ; Magnetic Resonance Spectroscopy ; Plant Roots ; chemistry ; Saponins ; chemistry ; isolation & purification