1.Determination of Ginsenoside Rb_1 in AITONG Capsules
Journal of Zhejiang Chinese Medical University 2006;0(02):-
[Objective] To establish n HPLC method for analysis of ginsenoside Rb1 in AITONG capsules. [Method]The HPLC system consists of G1314A variable wavelength un-visible detector,Hypersil ODS(4.6mm?250mm,5?m),HP chemstation, Hp1100 Series Quaternary Pump and Vacuum degasser (G1322A). The mobile phase was: Acetonitrile:Water (30∶70,v/v). The flowrate was 1.0ml?min-1,the injection volume was 20?l,and the detector wavelength was 203nm. [Results] The method was linear at the ginsenoside Rb1 ranging from 0.04?g to 2?g. The recovery of method was 98.26%(n=5),the average RSD was 1.41% .
2.Studies on quality standard of Aitong suppositoria
Chinese Journal of Modern Applied Pharmacy 2001;18(2):128-129
OBJECTIVE:Establish a method for the quality control of Ai tong suppositoria.METHOD:Borneolum,viverra were identifed by TLC.A m ethod of thin-layer UV spectrophotometry was used to determine the content of rh izoma wrydalis.RESULTS:The studies on the quality control showed tha t the characteristics for identification by TLC were distinct.The quantification method had the linear range of 0.5~25μg.The average recovery was 102.11% and I ts RSD was 1.12%.CONCLUSION:The methods for identificati on and quantification were simple,realizable.