1.Pharmacognostical identification of rhizomes of Costus L.
Chunfeng QIAO ; Luoshan XU ; Hui DONG ; Zhengtao WANG
Chinese Traditional and Herbal Drugs 1994;0(01):-
Object To provide a basis for the identification and quality control of the crud drugs of Costus L.. Methods Morphological and histological characters of the rhizomes of Costus spectosus (Koen.) Smith, Costus lacerus Gagnep.and Costus tonkinensis Gagnep. were described and illustrated, respectively. TLC of the above drugs was finished. Microscopical characters of the epidemis of leaves of these species were also compared. Results The characters involving the vessel order in vascular bundle ring at the inner side of pericycle in the transverse section, calcium oxalate crystals occurred in the vessel, the characteristic calcium oxalate crystals in the cortex and cork cell and the TLC qualitative analysis for diosgenin, etc. are important for identification of Costus L.. Conclusion These three crude drugs can be identified by the above research results.
2.Quality standard for Ershiwuwei Feibing Pills
Xiang LI ; Yali LIU ; Pei QIAO ; Jing ZHANG ; Zhiqing LIU ; Qin HUANG ; Jing CHEN ; Chunfeng ZHAN
Chinese Traditional Patent Medicine 2017;39(7):1410-1414
AIM To establish the quality standard for Tibeten medicine Ershiwuwei Feibing Pills [Inula racemosa Hook.f.,Swertia bimaculata (Sieb.et Zucc.) Hook.Thors.ex Clarke,Phyllanthus emblica Linn.,Terminalia billerica (Gaertn.) Roxb.,etc.].METHODS TLC was applied to the qualitative identification of L racemosa,S.bimaculata,P.emblica and T.billerica,and HPLC was adopted in the quantitative determination of alantolactone,oleanolic acid,gallic acid and hydroxysafflor yellow A.RESULTS The TLC spots were clear without negative interference.Alantolactone,oleanolic acid,gallic acid and hydroxysafflor yellow A showed good linear relationships within the ranges of 4.324-216.2 μg/mL (r =0.999 9),32.222-1 611.1 μg/mL (r =0.999 9),4.072-203.6 μg/mL (r =0.999 9) and 4.266-213.3 μg/mL (r =0.999 9),whose average recoveries (RSDs) were 100.6% (0.93%),100.3% (2.1%),101.5% (3.0%) and 100.1% (1.8%),respectively.CONCLUSION This simple method can be used for the rapid quality control of Ershiwuwei Feibing Pills.