PURPOSE: This study evaluated the bond strength between porcelain denture teeth (Bioblend 43D) and four different polymerized denture resins (Lucitone 199, Palapress, Acron MC, Triad) with and without a bonding agent and after four different types of surface treatment (polished, HF etched, sandblasted, air-abraded). MATERIALS AND METHODS: Central incisor porcelain denture teeth were divided into 32 groups of 5 each. Tensile bond strength (MPa) was determined using a testing machine at crosshead speed of 0.5 mm/min. Mean and standard deviation are listed. Data were analyzed by two-way ANOVA. Means were compared by Tukey-Kramer intervals at 0.05 significance level. RESULTS: All surface treatment increased bond strength compared to polished surface and the highest bond strength was found with Palapress resin with etched porcelain surface (8.1 MPa). Bonding agent improved the bond strength of all denture resins to porcelain teeth. Superior bonding was found with Palapress and air-abraded porcelain (39 MPa). CONCLUSION: Resins with different curing methods affect the bond strength of porcelain teeth to denture bases. Superior bonding was found with auto-polymerized resin (Palapress). Application of ceramic primer and bonding agent to porcelain teeth with and without surface treatment will improve the bond strength of all denture resins to porcelain teeth.
Acrylic Resins ; Ceramics ; Dental Porcelain* ; Denture Bases ; Dentures* ; Incisor ; Methods ; Polymers ; Polymethyl Methacrylate ; Tooth*

No abstract available.
Acrylic Resins ; Breast ; Hydrogel

PURPOSE: A new light curing urethane dimethacrylate and a cold curing resin with simpler and faster laboratory procedures may have even improved flexural properties. This study investigated the 3-point flexural strengths and flexural moduli of two alternate base materials. MATERIALS AND METHODS: A cold curing resin (Weropress) and a light curing urethane dimethacrylate base material (Eclipse). Along with Eclipse and Weropress, a high impact resin (Lucitone199) and three conventional base materials (QC 20, Meliodent and Paladent 20) were tested. A 3-point bending test was used to determine the flexural strengths and flexural moduli. The mean displacement, maximum load, flexural modulus and flexural strength values and standard deviations for each group were analyzed by means of one-way analysis of variance (ANOVA) (with mean difference significant at the 0.05 level). Post hoc analyses (Scheffe test) were carried out to determine the differences between the groups at a confidence level of 95%. RESULTS: Flexural strength, displacement and force maximum load values of Eclipse were significantly different from other base materials. Displacement values of QC 20 were significantly different from Lucitone 199 and Weropress. CONCLUSION: The flexural properties and simpler processing technique of Eclipse system presents an advantageous alternative to conventional base resins and Weropress offers another simple laboratory technique.
Acrylic Resins ; Cold Temperature ; Denture Bases ; Dentures ; Displacement (Psychology) ; Light ; Methacrylates ; Methylmethacrylates ; Polyurethanes ; Urethane

PURPOSE: The purpose of this study was to investigate the diametral tensile strength of polymer-based temporary crown and fixed partial denture (FPD) materials, and the change of the diametral tensile strength with time. MATERIAL AND METHODS: One monomethacrylate-based temporary crown and FPD material (Trim) and three dimethacrylate-based ones (Protemp 3 Garant, Temphase, Luxtemp) were investigated. 20 specimens (the empty set 4 mm x 6 mm) were fabricated and randomly divided into two groups (Group I: Immediately, Group II: 1 hour) according to the measurement time after completion of mixing. Universal Testing Machine was used to load the specimens at a cross-head speed of 0.5 mm/min. The data were analyzed using one-way ANOVA, the multiple comparison Scheffe test and independent sample t test (alpha = 0.05). RESULTS: Trim showed severe permanent deformation without an obvious fracture during loading at both times. There were statistically significant differences among the dimethacrylate-based materials. The dimethacrylate-based materials presented an increase in strength from 5 minutes to 1 hour and were as follows: Protemp 3 Garant (23.16 - 37.6 MPa), Temphase (22.27 - 28.08 MPa), Luxatemp (14.46 - 20.59 MPa). Protemp 3 Garant showed the highest value. CONCLUSION: The dimethacrylate-based temporary materials tested were stronger in diametral tensile strength than the monomethacrylate-based one. The diametral tensile strength of the materials investigated increased with time.
Acrylic Resins ; Bisphenol A-Glycidyl Methacrylate ; Collodion ; Composite Resins ; Crowns ; Denture, Partial, Fixed ; Methacrylates ; Polymethacrylic Acids ; Tensile Strength

PURPOSE: Polymethyl methacrylate (PMMA) is the most commonly used denture base material despite typically low in strength. The purpose of this study was to improve the physical properties of the PMMA based denture base resins (QC-20, Dentsply Ltd., Addlestone, UK; Stellon, AD International Ltd, Dentsply, Switzerland; Acron MC; GC Lab Technologies Inc., Alsip, Japan) by copolymerization mechanism. MATERIALS AND METHODS: Control group specimens were prepared according to the manufacturer recommendations. In the copolymer groups; resins were prepared with 5%, 10%, 15% and 20% acrylamide (AAm) (Merck, Hohenbrunn, Germany) content according to the moleculer weight ratio, respectively. Chemical structure was characterized by a Bruker Vertex-70 Fourier transform infrared spectroscopy (FTIR) (Bruker Optics Inc., Ettlingen, Germany). Hardness was determined using an universal hardness tester (Struers Duramin, Struers A/S, Ballerup, Denmark) equipped with a Vickers diamond penetrator. The glass transition temperature (Tg) of control and copolymers were evaluated by Perkin Elmer Diamond DSC (Perkin Elmer, Massachusetts,USA). Statistical analyses were carried out using the statistical package SPSS for Windows, version 15.0 (SPSS, Chicago, IL, USA). The results were tested regarding the normality of distribution with the Shapiro Wilk test. Data were analyzed using ANOVA with post-hoc Tukey test (P<.01). RESULTS: The copolymer synthesis was confirmed by FTIR spectroscopy. Glass transition temperature of the copolymer groups were higher than the control groups of the resins. The 10%, 15% and 20% copolymer groups of Stellon presented significantly higher than the control group in terms of hardness. 15% and 20% copolymer groups of Acron MC showed significantly higher hardness values when compared to the control group of the resin. Acrylamide addition did not affect the hardness of the QC-20 resin significantly. CONCLUSION: Within the limitation of this study, it can be concluded that copolymerization of PMMA with AAm increased the hardness value and glass transition temperature of PMMA denture base resins.
Acrylamide ; Acrylic Resins ; Chicago ; Collodion ; Denture Bases ; Dentures ; Diamond ; Glass ; Hardness ; Hardness Tests ; Polymethyl Methacrylate ; Pyridines ; Spectroscopy, Fourier Transform Infrared ; Spectrum Analysis ; Thiazoles ; Transition Temperature

PURPOSE: To evaluate changes over time of the anterior capsule opening size after phacoemulsification, based on haptic number and composition of three acrylic intraocular lenses (IOLs). METHODS: Fifty-five patients (70 eyes) were included. All underwent phacoemulsification followed by implantation of either an acrylic IOL with two-haptic (one-piece, 26 eyes; three-piece, 22 eyes), or four-haptic (one-piece, 22 eyes). The area of the anterior capsule opening size was measured one week postoperatively (baseline) and at three months. RESULTS: There was a significant reduction in the area of the anterior capsule opening from one week as compared to three months postoperatively in all groups (p < 0.001). However, there was no significant difference in the reduction in the anterior capsule opening between the IOLs (p = 0.36). CONCLUSIONS: The number and material of the haptic of the three acrylic IOLs did not influence the degree of anterior capsule opening shrinkage.
*Acrylic Resins ; Aged ; Cataract Extraction/*methods ; Female ; Follow-Up Studies ; Humans ; Lens Capsule, Crystalline/*physiopathology ; *Lenses, Intraocular ; Male ; *Polymethyl Methacrylate ; Postoperative Period ; Prosthesis Design ; Retrospective Studies ; *Silicone Elastomers

Poly (acrylic ester) hydrogel materials were widely used in intraocular lens and contact lens because of their excellent optical performance and biocompatibility. In this paper, the bulk copolymerization behavior of hydrophilic hydroxyethyl methacrylat with hydrophobic methyl metharylate was studied; and the optical performance, calcium deposits, equilibrium water content of polymers and its hydrogels obtained by different ratios of monomers were systematically investigated. The experimental results showed that the average light transmittance and the equilibrium water content of the obtained hydrogels increased with the increasing of the hydrophilic monomer content from 0 to 100%; however, the hardness decreased. The highest light transmittance reached 97% and the hardness of Shore A fell from 92 to 25, the equilibrium water content of hydrogel increased from 16% to 64%. The absorbent capacity of copolymers reduced with the adding of cross-linking monomer. When m(hydrophilic monomer): m(hydrophobic monomer) = 90 : 10, the combination property of the polymer and its hydrogel obtained is optimum.
Acrylic Resins ; chemical synthesis ; chemistry ; Biocompatible Materials ; chemical synthesis ; chemistry ; Humans ; Hydrogels ; chemical synthesis ; chemistry ; Lenses, Intraocular ; Polyhydroxyethyl Methacrylate ; chemical synthesis ; chemistry ; Tensile Strength

The purpose of this study was to investigate the physical effect of tissue conditioner on polymerized acrylic resins. Surface hardness and transverse strength were measured for evaluating physical effect of tissue conditioner on polymerized acrylic resins. 1) To measured surface hardness, the resin specimens(65x10x10mm size) of each resin material were made, applied tissue conditioner, stored in 37degrees C water for 1week, and changed tissue conditioner every week for 3 weeks. Surface hardness was measured every week with Shore hardness tester for 4 weeks. 2) To measured transverse strength, the resin specimens(65x10x3mm size & 65x10x1.5mm) of each resin material were made. The specimens were divided into four groups, and measured by universial testing machine. Group I (control group) : The resin specimens were stored in 37degrees C water for 5 weeks. Group II : The resin specimens were stored in 37degrees C water for 5 weeks, and relined in 1.5mm thickness with same resin. Group III : The resin specimens were stored in 37degrees C water for 1 week, applied tissue conditioner in 1.5mm thickness, stored in 37degrees C water for 1 week, changed tissue conditioner and water every week for 3 weeks, removed tissue conditioner, reduced 1.5mm thickness from resin surface which was applied tissue conditioner, and relined in 1.5mm thickness with same resin. The following conclusions were obtained : 1. Surface hardness changes of Vertex RS and Vertex SC were not different significantly (p>0.01). 2. Surface hardness of K-33, Tokuso rebase, and Kooliner were decreased (p<0.01). 3. With the exception of Kooliner, transverse strength of all resin materials between control group and groups which applied with tissue conditioner were not different significantly (p>0.01).
Acrylic Resins* ; Hardness ; Hardness Tests ; Polymers* ; Water

A variety of dermal fillers is available and has been used for soft tissue augmentation. Fillers used in rhinoplasty are minimally invasive and can help patients who are concerned with surgical procedures and recovery time. Nevertheless, there have been many reports about unsatisfactory results and complications using fillers for augmentation rhinoplasty. The unsatisfactory results include ill defined lateral aspect of nose, widening of injected filler, migration, and overcorrection. Therefore, the filler materials should be used according to its properties and nasal anatomical characteristics.
Acrylic Resins ; Humans ; Hyaluronic Acid ; Nose ; Rhinoplasty

This study aims to improve the solubility and bioavailability of daidzein by preparing the β-cyclodextrin-daidzein/PEG_(20000)/Carbomer_(940) nanocrystals. Specifically, the nanocrystals were prepared with daidzein as a model drug, PEG_(20000), Carbomer_(940), and NaOH as a plasticizer, a gelling agent, and a crosslinking agent, respectively. A two-step method was employed to prepare the β-cyclodextrin-daidzein/PEG_(20000)/Carbomer_(940) nanocystals. First, the insoluble drug daidzein was embedded in β-cyclodextrin to form inclusion complexes, which were then encapsulated in the PEG_(20000)/Carbomer_(940) nanocrystals. The optimal mass fraction of NaOH was determined as 0.8% by the drug release rate, redispersability, SEM morphology, encapsulation rate, and drug loading. The inclusion status of daidzein nanocrystals was determined by Fourier transform infrared spectroscopy(FTIR), thermogravimetric analysis(TGA), and X-ray diffraction(XRD) analysis to verify the feasibility of the preparation. The prepared nanocrystals showed the average Zeta potential of(-30.77±0.15)mV and(-37.47±0.64)mV and the particle sizes of(333.60±3.81)nm and(544.60±7.66)nm before and after daidzein loading, respectively. The irregular distribution of nanocrystals before and after daidzein loading was observed under SEM. The redispersability experiment showed high dispersion efficiency of the nanocrystals. The in vitro dissolution rate of nanocrystals in intestinal fluid was significantly faster than that of daidzein, and followed the first-order drug release kinetic model. XRD, FTIR, and TGA were employed to determine the polycrystalline properties, drug loading, and thermal stability of the nanocrystals before and after drug loading. The nanocrystals loaded with daidzein demonstrated obvious antibacterial effect. The nanocrystals had more significant inhibitory effects on Staphylococcus aureus, Escherichia coli, and Pseudomonas aeruginosa than daidzein because of the improved solubility of daidzein. The prepared nanocrystals can significantly increase the dissolution rate and oral bioavailability of the insoluble drug daidzein.
Sodium Hydroxide ; Acrylic Resins ; Escherichia coli ; Nanoparticles