1.Determination of Trace Organic Pollutants in Drinking Water by Solid-Phase Extraction Gas Chromatography-Mass Spectrometry
Yemei YANG ; Fengming ZHU ; Xuexian ZOU
Journal of Environment and Health 1993;0(01):-
Objective To develop a method for determination of trace organic pollutants in drinking water. Methods The organic pollutants in water were enriched and separated by a solid-phase extraction method with the big form resin of hole pattern as the enrichment of stationary phase and then were detected by GC-MS. Results The ideal test condition and the enriched method of sample were established in the present paper. Many water samples were determined by the newly established method. Over 100 organic pollutants were identified in these samples. Conclusion The newly established method is simple, fast, sensitive and easy to popularize and is suitable for determining organic chemical compounds in tap water, clean underground water and the water of source water.
2.Clinical Investigation of Concentration of Lidocaine in Intravenous Combining Anesthesia with GaS Chromatography
Zhiqing MO ; Guangyu ZHAO ; Lifang CHEN ; Xian KUANG ; Lu ZHANG ; Xuexian ZOU
Journal of Kunming Medical University 1988;0(03):-
The purpose of this paper was to find a safe and effective concentration of lido- caine in intravenous combining anesthesia.33 cases had been maintained with the intravenous instillation of 0.5% lidocaine and 0.1% scotine the lidocaine concentrations at the period of after introduction,30',60',90',120'and recovery were measured respectively.The safty and effective range of this drug would be 2.1—5?g/ml. Also,in this paper,the relationship between the rate of instilation and the concentration of Lidocaine was studied.There was a positive correlation between the drope per minute amd the concentration during the period of the first 60 minutes. After 90 minutes from the beginning,there was no linear correlation.If we want to maintain the safty and effective blood concentration(2.1—5?g/ml), the necessary rate of instillation is 46?10 drops/minute during the first 60 minutes and 27.8?5 drops/minute after 90 minutes.This result shows that lidocaine is easy to accumulate obviously in the body.If we want the patient to recover at the time of the operation just performed,we must stop this drug 50 miuutes before the operation is finished.