1.Flexural and compressive properties of layered specimens formed with flowable and composite resins
Jang Hoon LEE ; Seung Seo KIM ; Hyo Joung SEOL ; Yong Hoon KWON
Korean Journal of Dental Materials 2018;45(2):129-138
Flowable resins can be used as a base material during the restoration of deep tooth cavity. The purpose of the present study was to evaluate the mechanical properties of the layered specimens which have flowable resin as a base material. For the study, two composite resins and five flowable resins were chosen for the overlying and base materials, respectively. Flexural and compressive properties of each bulk and ten layered specimens were measured. Layered specimens showed high flexural strength (FS) and flexural modulus (FM) if bulk state FS and FM of the base flowable resin are high. However, compressive strength (CS) was not that case. CS of the layered specimen was not high (251.4~295.3 MPa) whether CS of the bulk state is high or not (259.8~439.8 MPa). FM showed high linear correlation with CM. After all mechanical properties of the layered specimens were not consistently influenced by the mechanical properties of the base flowable resins regardless of the overlying composite resins.
Composite Resins
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Compressive Strength
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Tooth
2.Tensile bond strength of four porcelain repair systems.
Young A JEON ; Byung Duk YANG ; Ho Jin LEE ; Ju Mi PARK ; Kwang Yeob SONG
The Journal of Korean Academy of Prosthodontics 2005;43(2):149-157
STATEMENT OF PROBLEM: Dental ceramics exhibit excellent esthetic property, compressive strength, chemical durability, biocompatibility and translucency. However, it suffers from inherent brittle fractures. Various techniques and materials for intraoral porcelain repair has been suggested. PURPOSE: This study is to compare the tensile bond strength of four commonly used porcelain repair systems (Vivadent, Bisco, Ultradent, Voco) and to insure the best system for the clinical application to the fractured porcelain. MATERIALS AND METHODS: A total of fifty specimens were fabricated. Specimens were stored in 37degrees C distilled water for 7 days and thermocycling was performed(1000 cycles), and subjected to a tensile force parallel to the repair resin and porcelain interface by use of an Universal Testing Machine. RESULT: 1. Voco showed the highest tensile bond strength. In decreasing order, the tensile bond strength of the other materials was as follows : Ultradent, Bisco, Vivadent. 2. There was a statistically significant difference between the porcelain repair systems(Voco, Ultradent > Bisco, Vivadent) (p<0.05). 3. SEM examination of prepared porcelain surfaces revealed that the surface treated with Voco showed brittle fracture. However, Ultradent, Bisco and Vivadent showed ductile fracture. 4. All specimens treated with four porcelain repair systems showed adhesive failure between porcelain and composite resin.
Adhesives
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Ceramics
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Compressive Strength
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Dental Porcelain*
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Water
3.Physical properties of a new resin-based root canal sealer in comparison with AH Plus Jet.
Myint THU ; Jin Woo KIM ; Se Hee PARK ; Kyung Mo CHO
Journal of Dental Rehabilitation and Applied Science 2017;33(2):80-87
PURPOSE: The aim of this study was to assess the physical properties of a novel resin-based endodontic sealer, Any-Seal, in comparison with AH Plus Jet. MATERIALS AND METHODS: Flow, radiopacity and compressive strength were examined according to ISO 6876/2001. For flow test, 0.05 mL of sealer was placed between glass plate and 100 g weight were applied. Ten minutes after mixing the sealers, the load was removed and the diameters of the compressed sealer discs were measured. For radiopacity, 10 mm diameter and 1 mm thickness sample were fabricated and took radiograph with an aluminum step-wedge and analyzed using imaging program. For compressive strength test, 4 mm × 6 mm cylindrical specimen was fabricated and tested after 24 hours and 1 week using Universal testing machine. RESULTS: Both tested sealers were consistent with ISO 6876/2001 in the flow and radiopacity test. The flow values of both sealers were not significantly different (P > 0.05). AH Plus Jet had significantly higher radiopacity (P < 0.05). AH Plus Jet showed higher compressive strength at both time intervals (P < 0.05). CONCLUSION: Any-Seal showed low compressive strength until after 1 week, so its physical and biological aspect should be evaluated more before clinical use.
Aluminum
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Compressive Strength
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Dental Pulp Cavity*
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Glass
4.A new mathematical equation for the evaluation of the compression behavior of pharmaceutical materials.
Sheng-jun CHEN ; Jia-bi ZHU ; Xiao-le QI
Acta Pharmaceutica Sinica 2012;47(10):1384-1388
A new mathematical equation characterizing the compression of pharmaceutical materials is presented. This equation presumed that the rate of change of the compressible volume of powder with respect to the pressure is proportional to the compressible volume. The new model provided a good fit to several model substances employing non-linear regression techniques. The validity of the model had been verified with experimental results of various pharmaceutical powders according to the Akaikes informatics criterion (AIC) and the sum of squared deviations (SS). The parameter of the new model might reflect quantitatively the fundamental compression behaviors of the powders. It had demonstrated that the proposed model could well predict the compaction characteristics of solid particles like the Kawakita model.
Compressive Strength
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Nonlinear Dynamics
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Powders
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chemistry
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Pressure
5.A comparative study on cyclic and static fatigue of dental ceramic by means of Hertzian's contact.
Wei-cai LIU ; Yong-lie CHAO ; Qian-bing WAN ; Cheng-min HUANG
Chinese Journal of Stomatology 2005;40(6):508-510
OBJECTIVETo compare the difference in strength degradation and morphology damage of brittle dental ceramic after static load and cyclic fatigue.
METHODSHertzian's contact technique with a tungsten carbide sphere was used to investigate the response of feldspathic dental porcelain to static load and cyclic fatigue. All specimens were subjected to static or cyclic loading in moist environment. Furthermore the surviving strength of specimens was examined by the three-point test and the morphology damage was observed. Statistical analyses were performed with ANOVA and a P-value less than 0.05 was considered to be significant.
RESULTSOuter cone crack and associated strength degradation simultaneously occurred both after the first cyclic loading and static loading. Up to 1,000 cycles, the specimens showed inner cone cracks and strength degradation was aggravated. No significant difference in the strength degradation among all static loading specimens and no inner cone cracks occurred in static loading specimens.
CONCLUSIONSBoth static and cyclic fatigue influence dental ceramic strength, but cyclic fatigue is more deleterious.
Compressive Strength ; Dental Porcelain ; Materials Testing
6.Effect of different veneering techniques on the fracture strength of metal and zirconia frameworks.
Ayse Gozde TURK ; Mubin ULUSOY ; Mert YUCE ; Hakan AKIN
The Journal of Advanced Prosthodontics 2015;7(6):454-459
PURPOSE: To determine whether the fracture strengths and failure types differed between metal and zirconia frameworks veneered with pressable or layering ceramics. MATERIALS AND METHODS: A phantom molar tooth was prepared and duplicated in 40 cobalt-chromium abutments. Twenty metal (IPS d.SIGN 15, Ivoclar, Vivadent, Schaan, Liechtenstein) and 20 zirconia (IPS e.max ZirCAD, Ivoclar) frameworks were fabricated on the abutments. Each framework group was randomly divided into 2 subgroups according to the veneering material: pressable and layering ceramics (n=10). Forty molar crowns were fabricated, cemented onto the corresponding abutments and then thermocycled (5-55degrees C, 10,000 cycles). A load was applied in a universal testing machine until a fracture occurred on the crowns. In addition, failure types were examined using a stereomicroscope. Fracture load data were analyzed using one-way ANOVA and Tukey HSD post-hoc tests at a significance level of 0.05. RESULTS: The highest strength value was seen in metal-pressable (MP) group, whereas zirconia-pressable (ZP) group exhibited the lowest one. Moreover, group MP showed significantly higher fracture loads than group ZP (P=.015) and zirconia-layering (ZL) (P=.038) group. No significant difference in fracture strength was detected between groups MP and ML, and groups ZP and ZL (P>.05). Predominant fracture types were cohesive for metal groups and adhesive for zirconia groups. CONCLUSION: Fracture strength of a restoration with a metal or a zirconia framework was independent of the veneering techniques. However, the pressing technique over metal frameworks resisted significantly higher fracture loads than zirconia frameworks.
Adhesives
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Ceramics
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Compressive Strength
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Crowns
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Dental Porcelain
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Molar
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Tooth
7.Mechanical properties and microleakage of composite resin materials cured by variable light intensities.
Seung Ryul HAN ; Kyung San MIN ; Dong Hoon SHIN
Journal of Korean Academy of Conservative Dentistry 2003;28(2):134-145
Mechanical properties and microleakage of two composites [conventional hybrid type DenFil (VERICOM Co., Anyang, Korea) / micro matrix hybrid type Esthet X (Dentsply Caulk, Milford, DE, U.S.A.)] were evaluated to assess whether variable light intensity curing is better than conventional curing technique. Curing was done for 40 seconds in two ways of 2 step soft-start technique and 5 step ramping technique. Three kinds of light intensities of 50, 100, 200 mW/cm2 were initially used for 10, 20, 30 seconds each and the maximum intensity of 600 mW/cm2 was used for the rest of curing time in a soft-start curing technique. In a ramping technique, curing was done with the same initial intensities and the light intensity was increased 5 times with the same rate to the maximum intensity of 600 mW/cm2. After determining conditions that showed no different mechanical properties with conventional technique, Esthet X composite was filled in a class V cavity, which dimension was 4x3x1.5 mm and cured under those conditions. Microleakage was evaluated in two ways of dye penetration and maximum gap estimation through SEM observation. ANOVA and Spearman's rho test were used to confirm any statistical significance among groups. The results were as follows: 1. Several curing conditions of variable light intensities resulted in the similar mechanical properties with a conventional continuous curing technique, except conditions that start curing with an initial light intensity of 50 mW/cm2, 2. Conventional and ramping techniques were better than soft-start technique in mechanical properties of microhardness and compressive strength. 3. Soft-start group that started curing with an initial light intensity of 100 mW/cm2 for 10 seconds showed the least dye penetration. Soft-start group that started curing with an initial light intensity of 200 mW/cm2 for 10 seconds showed the smallest marginal gap, if there was no difference among groups. 4. Soft-start technique resulted in better dye-proof margin than conventional technique (p=0.014) and ramping technique(p=0.002). 5. There was a very low relationship(p=0.157) between the methods of dye penetration and marginal gap determination through SEM evaluation. From the results of this study, it was revealed that ramping technique would be better than conventional technique in mechanical properties, however, soft-start technique might be better than conventional one in microleakage. It was concluded that much endeavor should be made to find out the curing conditions, which have advantages of both aspects or to solve these kinds of problems through a novel idea of polymerization.
Architectural Accessibility
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Compressive Strength
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Gyeonggi-do
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Polymerization
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Polymers
8.The effect of the thread depth on the mechanical properties of the dental implant.
Sun Young LEE ; Sung Jun KIM ; Hyun Wook AN ; Hyun Seung KIM ; Dong Guk HA ; Kyung Ho RYO ; Kwang Bum PARK
The Journal of Advanced Prosthodontics 2015;7(2):115-121
PURPOSE: This study aimed to evaluate the effect of implant thread depth on primary stability in low density bone. MATERIALS AND METHODS: The insertion torque was measured by inserting Ti implants with different thread depths into solid rigid polyurethane blocks (Sawbones) with three different bone densities (0.16 g/cm3, 0.24 g/cm3, and 0.32 g/cm3). The insertion torque value was evaluated with a surgical engine. The static compressive strength was measured with a universal testing machine (UTM) and the Ti implants were aligned at 30degrees against the loading direction of the UTM. After the static compressive strength test, the Ti implants were analyzed with a Measurescope. RESULTS: The Ti implants with deeper thread depth showed statistically higher mean insertion torque values (P<.001). Groups A and group B had similar maximum static compressive strengths, as did groups C and D (P>.05). After the static compressive strength, the thread shape of the Ti implants with deeper thread depth did not show any breakage but did show deformation of the implant body and abutment. CONCLUSION: The implants with deeper thread depth had higher mean insertion torque values but not lower compressive strength. The deep threads had a mechanical stability. Implants with deeper thread depth may increase the primary stability in areas of poor quality bone without decreasing mechanical strength.
Bone Density
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Compressive Strength
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Dental Implants*
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Polyurethanes
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Torque
9.The effect of the thread depth on the mechanical properties of the dental implant.
Sun Young LEE ; Sung Jun KIM ; Hyun Wook AN ; Hyun Seung KIM ; Dong Guk HA ; Kyung Ho RYO ; Kwang Bum PARK
The Journal of Advanced Prosthodontics 2015;7(2):115-121
PURPOSE: This study aimed to evaluate the effect of implant thread depth on primary stability in low density bone. MATERIALS AND METHODS: The insertion torque was measured by inserting Ti implants with different thread depths into solid rigid polyurethane blocks (Sawbones) with three different bone densities (0.16 g/cm3, 0.24 g/cm3, and 0.32 g/cm3). The insertion torque value was evaluated with a surgical engine. The static compressive strength was measured with a universal testing machine (UTM) and the Ti implants were aligned at 30degrees against the loading direction of the UTM. After the static compressive strength test, the Ti implants were analyzed with a Measurescope. RESULTS: The Ti implants with deeper thread depth showed statistically higher mean insertion torque values (P<.001). Groups A and group B had similar maximum static compressive strengths, as did groups C and D (P>.05). After the static compressive strength, the thread shape of the Ti implants with deeper thread depth did not show any breakage but did show deformation of the implant body and abutment. CONCLUSION: The implants with deeper thread depth had higher mean insertion torque values but not lower compressive strength. The deep threads had a mechanical stability. Implants with deeper thread depth may increase the primary stability in areas of poor quality bone without decreasing mechanical strength.
Bone Density
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Compressive Strength
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Dental Implants*
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Polyurethanes
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Torque
10.Study on some mechanism of leucite microcrystallization to reinforce dental glass ceramics.
Biao ZHANG ; Fatang QIAN ; Xinglong DUAN ; Bolin WU
Chinese Journal of Stomatology 2002;37(4):260-264
OBJECTIVETo research the influence of K(2)O composition in the raw material on leucite microcrystallization and to study the effect of leucite content on compressive strength of the dental glass ceramics reinforced by leucite microcrystallization.
METHODSThe raw materials with different K(2)O content were treated by a decided thermal treatment system. The products were analyzed by polaring microscope and X-ray diffractometer, and their compressive strength was also tested.
RESULTSThe microstructure of products from high K(2)O component was remarkably good, at microcrystal size of 0.8 micro m and the compressive strength was 206.6 MPa. A positive correlation was found between leucite volume and the compressive strength when leucite volume was less than 50% (Vol%).
CONCLUSIONSThe component of K(2)O has a great effect on the microstructure and the properties of the leucite-microcrystal-reinforced dental glass ceramics and the content of leucite microcrystals has a notable influence on the compressive strength of the dental glass ceramics.
Compressive Strength ; Crystallization ; Dental Porcelain ; chemistry ; Glass ; chemistry ; Materials Testing