1.The clinical observation and the nursing countermeasures about using the TR band to stop blooding
Xuejun JIANG ; Jian LIN ; Aimei TAN ; Xuelong ZHANG ; Weilan QIU ; Xingfei RUAN ; Yu LU
Chinese Journal of Practical Nursing 2006;0(24):-
Objective To evaluate the clinical values of the TR band, analyze the factors about the hemorrhage delay at the same time. Methods Divided 98 patients who had accepted the radial artery interventional radiology into the observation group (52 cases) and the control group (46 cases) randomly. The TR band was used in the observation group and the routine nursing method was used in the control group. Results The incidence rate of complication in the observation group was significant lower than that of in the control group,P
2.Establishment of hydride generation atomic fluorescence spectrometry for the determination of arsenic and selenium in hair
Aimei BAI ; Yue LI ; Wenhong TAN
Chinese Journal of Endemiology 2018;37(6):509-512
Objective To establish a method for simultaneous determination of arsenic and selenium in hair by hydride generation atomic fluorescence spectrometry.Methods The A and B of the hair samples were digested via the wet method,and the arsenic and selenium contents were determined simultaneously with a dual channel atomic fluorescence spectrophotometer.Standard blank solution was continuously determined for 11 times,the detection limit was calculated according to the blank solution three times the standard deviation.Hair samples A and B were continuously determined for 11 times,and the precision was determined according to the coefficient of variation (CV).The hair samples C and D were did 11 times of standard addition experiment,the standard added was close to the sample low value.The accuracy was determined by the standard recovery rate.Results The lowest detection limits of arsenic and selenium were 0.081,0.036 μg/L,the precisions of arsenic and selenium in sample A were (0.694 9 ± 0.024 2) and (1.930 2 ± 0.098 5) μg/g,the CV were 3.54% and 5.09%.The precisions of arsenic and selenium in sample B were (6.212 2 ± 0.137 3) and (8.282 2 ± 0.266 8) μg/g,the CV were 2.21% and 3.22%;the recovery rates of sample C of arsenic and selenium were 96.30% ~ 110.00% and 94.80% ~ 110.00%;the recovery rates of sample D of arsenic and selenium were 93.63% ~ 108.20% and 97.03% ~ 108.34%.Conclusions The method using hydride atomic fluorescence for determination of arsenic and selenium in the hair has been successfully established.This method is simple and easy to operate,with high sensitivity and good accuracy and precision,high recovery,less matrix interference,and less reagent consumed etc.It is worth promoting in prevention and control of endemic diseases.