Determination of scopolamine in the poisoning case by GC/MS.
- Author:
Jian-Xin CHU
1
;
Yu XIE
;
Xiao-Cong ZHUO
Author Information
1. The Procuratorate of Zhejiang Province, Hangzhou 310012, China.
- Publication Type:Journal Article
- MeSH:
Foodborne Diseases/etiology*;
Forensic Medicine/methods*;
Gas Chromatography-Mass Spectrometry/methods*;
Hallucinations/diagnosis*;
Humans;
Male;
Psychoses, Substance-Induced/etiology*;
Scopolamine/poisoning*;
Sensitivity and Specificity;
Solanaceae/chemistry*;
Solvents/chemistry*
- From:
Journal of Forensic Medicine
2006;22(4):285-287
- CountryChina
- Language:Chinese
-
Abstract:
OBJECTIVE:To separate and determine scopolamine from the food in a poisoning case by GC/MS.
METHODS:The scopolamine was determined by GC/MS/El used CP5860(CP-sil8CB) column (30 mx 0.25 mmx 0.33 microm) with liquid- liquid extraction.
RESULTS:The deny scopolamine was found in the case sample, and the chromatographic separation of the peaks is fine.
CONCLUSION:The method is accurate and reliable.