Glycoside constituents from Bletilla striata
10.7501/j.issn.0253-2670.2019.20.006
- VernacularTitle: 黔产白及中糖苷类化学成分研究
- Author:
Chang-Fen CHEN
1
Author Information
1. State Key Laboratory of Functions and Applications of Medicinal Plants, Guizhou Medical University
- Publication Type:Journal Article
- Keywords:
1-methyl-3-phenylpropyl-β-D-glucopyranoside;
4-methylphenyl-β-D- glucopyranoside;
Bletilla striata (Thunb.) Reichb. f.;
Gastrodin;
Glycoside
- From:
Chinese Traditional and Herbal Drugs
2019;50(20):4879-4883
- CountryChina
- Language:Chinese
-
Abstract:
Objective: To study the glycoside chemical constituents of Bletilla striata grown in Guizhou Province. Methods: The glycoside chemical constituents were separated and purified by silica gel column chromatography, MCI, gel column chromatography, medium pressure preparation, highperformance liquid chromatography and other modern separation methods. The structures were identified based on the spectral data. Results: Thirteen glycosides were isolated from the 95% ethanol extracts: 1-methyl-3-phenylpropyl-β-D-glucopyranoside (1), 1-(4-β-D-glucopyranosyl oxybenzyl) 4-ethyl (2R)-2-isobutylmalate (2), 3’,5- dimethoxy-bibenzyl-3-O-β-D-glucopyranoside (3), syringaresinol mono-β-D-glucoside (4), 4-O-(6’-O-glucosyl-p-coumaroyl)-4- hydroxybenzyl alcohol (5), (4-hydroxyphenyl) methyl-β-D-glucopyranoside (6), 4-methylphenyl-β-D-glucopyranoside (7), benzyl-β-D- glucopyranoside (8), phenyl-β-D-glucopyranoside (9), 4-[(acetyloxy) methyl] phenyl-β-D-glucopyranoside (10), batatasin III-3-O- glucoside (11), gastrodin (12) and 4-(4-β-D-glucopyranosyl-oxybenzyl)-(2R)-2-isobutylmalate (13). Conclusion: Compound 1 is a new natural product. Compounds 3-6 are isolated from this plant for the first time; Compounds 2, 7-13 are obtained from this genus for the first time.