Comparison between pyrophosphate method and infrared spectrophotometry for determination of silicon dioxide content in dust
10.3760/cma.j.issn.1001-9391.2019.10.014
- VernacularTitle: 粉尘中二氧化硅测定的焦磷酸法和红外分光光度法比较
- Author:
Shulan ZHAO
1
;
Mengmeng LIU
;
Hao LI
;
Qiang ZENG
Author Information
1. Tianjin Centers for Disease Control and Prevention, Tianjin 300011, China
- Publication Type:Journal Article
- Keywords:
Dust;
Silicon dioxide;
Quartz;
Pyrophosphate method;
Spectrophotometry, infrared
- From:
Chinese Journal of Industrial Hygiene and Occupational Diseases
2019;37(10):781-784
- CountryChina
- Language:Chinese
-
Abstract:
Objective:To discuss the difference between pyrophosphoric acid method and infrared spectrophotometry for the determination of silica content in dust.
Methods:The content of silica in the laboratory comparison samples organized by CDC Occupational Health Institute in China in 2018, and purchased quality control samples were determined by pyrophosphate method. Meanwhile, the samples were qualitatively and quantitatively analyzed by infrared spectrophotometry, and the results obtained by the two methods were compared.
Results:Four samples (062C1、062C2、GDOHZKTG012-1、GDOHZKTG012-2) were detected by pyrophosphate method and infrared spectrophotometry. The results of pyrophosphate method were 55.49%, 5.24%, 4.90% and 54.72%, respectively. The results of infrared spectrophotometry were 0.91%, 1.87%, 1.29% and 1.16% respectively.
Conclusion:The content of silica in dust determined by pyrophosphate method is higher than that by infrared spectrophotometry.
