Study on quality standard of Baibu Zhike syrup
10.3969/j.issn.1006-0111.2018.01.015
- VernacularTitle:百部止咳糖浆的质量标准研究
- Author:
Rong QU
1
;
Yajing QIU
;
Ganggang BAI
;
Xiaopeng CHEN
;
Hui YE
Author Information
1. 泰州市食品药品检验所
- Keywords:
Baibu Zhike syrup;
Stemonae Radix;
Platycodonis Radix;
hesperidin;
quality standard
- From:
Journal of Pharmaceutical Practice
2018;36(1):71-74
- CountryChina
- Language:Chinese
-
Abstract:
Objective To establish the quality standard for Baibu Zhike syrup .Methods TLC method was used for qualitative identification of Stemonae Radix and Platycodonis Radix .The content of hesperidin in Citri Exocarpium Rubrum was determined by HPLC method on C18 column with mobile phase of acetonitrile-water (18:82) .The detection wavelength was 284 nm .Results The clear spots on TLC indicated a good separation with no interference to negative control .The linear range of hesperidin was 0 .0669-1 .6725μg (r=0 .9999) .The average recovery was 96 .6％ .Conclusion This method is sim-ple ,rapid and reproducible .It can be used for the quality control of Baibu Zhike syrup .
