Chemical constituents from the n-butanol fraction of Polygonum amplexicaule var.sinense
10.3969/j.issn.1001-1528.2018.03.024
- VernacularTitle:中华抱茎蓼正丁醇部位化学成分的研究
- Author:
Fan ZHAO
1
;
Zhe-Ming WANG
;
Bi-Qing ZHAO
;
Qun-Gang QIAN
;
Li LI
;
Wan DAI
;
Guang-Ming XU
;
Xiao-Jiang ZHOU
Author Information
1. 湖南中医药大学
- Keywords:
Polygonum amplexicaule var.sinense;
chemical constituents;
isolation and identification
- From:
Chinese Traditional Patent Medicine
2018;40(3):626-629
- CountryChina
- Language:Chinese
-
Abstract:
AIM To study the chemical constituents from the Polygonum amplexicaule var.sinense.METHODS The n-butanol fraction of ethanol extract from P.amplexicaule var.sinense was isolated and purified by TLC,normal-phase silica,macroporous resin column,sephadex column,preparative TLC and semi-preparative HPLC column,then the structures of obtained compounds were identified by physicochemical properties and spectral data.RESULTS Ten compounds were identified as 2-(aminomethyl)-4-methoxy-phenol (1),p-methyl-hydroxybenzoate (2),p-methyl-hydroxyphenylacetate (3),2-[2-(methylamino) phenyl]-4-thiazolecarboxylic acid,methyl ester (4),p-methylphenylethanol (5),bergenin (6),arbutin (7),rhododendron-2-O-β-D-glucopyranoside (8),n-butyl gallate (9) and β-sitosterol (10).CONCLUSION Compounds 1-8 are isolated from this plant for the first time.
