Analysis of Volatile Compounds Extracted from Dipsaci Radix and Its Wine Broiled Products by GC-MS
- VernacularTitle:气相色谱-质谱联用技术分析续断及其酒灸品中挥发性成分
- Author:
Hua LU
1
;
Yisheng ZHANG
;
Chen YI
;
Xin YE
;
Jinqing LU
Author Information
1. 武汉市中医医院药学部 武汉430014
- Keywords:
Dipsaci Radix;
wine broiled products;
Volatile components;
HS-SPME;
GC-MS
- From:
China Pharmacist
2018;21(10):1738-1742
- CountryChina
- Language:Chinese
-
Abstract:
Objective: To analyze the composition and the content of volatile components in Dipsaci Radix and its wine broiled products. Methods: Headspace solid phase microextraction (HS-SPME) combined with gas chromatography-mass spectrometry ( GC-MS) was used to analyze the volatile components in Dipsaci Radix and its wine broiled products. The area normalization method was used to calculate the relative content. Results: Totally 31 ingredients were identified, which mainly included phenols, olefins, alcohols and aldehydes. Totally 25 peaks were detected out from the volatile components in Dipsaci Radix, and among them, 22 components were identified, which accounted for 94. 74% of the total volatile components. The content of 5-allylguaiacol was the highest, which accounted for 28. 37% of the total volatile components. Totally 23 peaks were detected out from the volatile components in wine-pro-cessed Dipsaci Radix, and among them, 17 ingredients were identified, which accounted for 85. 92% of the total volatile components. The content of nonanal was the highest, which accounted for 9. 66% of the total volatile components. Conclusion: The composition and the content of volatile components in Dipsaci Radix and its wine broiled products are different. The experiment provides scientific reference for the further research and development of the volatile components in Dipsaci Radix and its wine broiled products.
