Determination of Sinapine in Semen Raphani
- VernacularTitle:莱菔子中芥子碱的含量测定
- Author:
Lifang LIU
;
Yuxin WANG
;
Xinyong ZHANG
;
Xuefang LIU
;
- Publication Type:Journal Article
- Keywords:
Semen Raphani;
sinapine;
HPLC
- From:
Chinese Traditional Patent Medicine
1992;0(01):-
- CountryChina
- Language:Chinese
-
Abstract:
Objective: To determine the sinapine in Semen Raphani(Laifuzi) from different places by measns of RP HPLC. Method: The column empolyed was Alltima Phenyl Collumn(250?4.6mm,5?m). The mobile phase was acetonitrile 0.08 mol/LKH 2PO 4(15∶85). The flow rate was 1.0mL/min and detection was effected at 326nm results. Conclusion: The results show the method is accurate, rapid and reproducible. We found it has marked discrepancy in the content of Semen Raphani(Lai Fuzi) from different places.
