Experimental studies on microwave-assisted extraction of baicalin from root of Scutellariae baicalensis
- VernacularTitle:黄芩中黄芩苷微波提取的实验研究
- Author:
Zhenku GUO
;
Qinhan JIN
;
Guoqiang FAN
;
Yuping DUAN
;
Chen QIN
;
- Publication Type:Journal Article
- Keywords:
microwave assisted extraction;
orthogonal test;
root of Scutellariae baicalensis Georgi;
baicalin
- From:
Chinese Traditional and Herbal Drugs
1994;0(11):-
- CountryChina
- Language:Chinese
-
Abstract:
Object To study the microwave assisted procedure for the extraction of baicalin from root of Scutellariae baicalensis Georgi Methods An MSP 100D domestically made microwave sample preparation system with a maximum power of 850 watts was used. The effects of solvents, pressure/temperature of solvents and microwave radiation time on the yield of baicalin were studied by orthogonal experimental design. Results The optimal experimental conditions were extraction at 70% of microwave power with 30 times of 35% ethanol at a constant heating pressure/temperature of 0.15 MPa for 30 s. Conclusion The microwave assisted extraction not only takes a shorter time with better parallel results, but also gave an increased yield of about 10% as compared with ultrasonic extraction.