Rapid Preparation of Micro-sized Gold Nanorods
10.11895/j.issn.0253-3820.170357
- VernacularTitle:小尺寸金纳米棒的快速制备及影响因素的研究
- Author:
Ling Jia ZHOU
1
;
Qian Qian DUAN
;
Wei Peng LI
;
Qun Ao JIAN
;
Long Jian JI
;
Qiang ZHANG
;
Bo Sheng SANG
Author Information
1. 太原理工大学信息工程学院 微纳系统研究中心
- Keywords:
Seedless growth method;
Micro-sized;
High aspect ratio;
Gold nanorods;
Mercury ion Ⅱ
- From:
Chinese Journal of Analytical Chemistry
2017;45(10):1482-1488
- CountryChina
- Language:Chinese
-
Abstract:
The effects of cetyltrimethylammonium bromide ( CTAB) , ascorbic acid, NaBH4 and AgNO3 , as well as the stirring time and reaction time on the preparation of gold nanorods synthesized with seedless growth method were studied. The optimum preparation conditions were obtained in the process of growth of gold nanorods. The gold nanorods prepared under different conditions were characterized by visible absorption spectroscopy and transmission electron microscopy ( TEM ) . Under the optimum conditions such as room temperature, 0. 1 mol/L CTAB, 96 μmol/L AgNO3 , 0. 97 mmol/L ascorbic acid, 1. 5 μmol/L NaBH4 and stirring for 25 s, micro-sized gold nanorods with uniform morphology, good dispersibility, small shaft width and high aspect ratio were prepared within 6 h. The gold nanorods were expected to be applied to the detection of mercury ion in water environment.
