The effects of magnetron-sputtered ZrSiN/ZrO2 gradient coating on the bonding strength of titanium to porcelain
10.3969/j.issn.1001-3733.2016.05.009
- VernacularTitle:磁控溅射ZrSiN/ZrO2复合梯度涂层纯钛表面对钛瓷结合强度的影响
- Author:
Xiaojing WANG
;
Guowei WANG
;
Guangyan HUI
;
Wenmin JIA
;
Yimin ZHAO
;
Tianwen GUO
- Keywords:
Magnetron sputtering;
ZrSiN/ZrO2;
Gradient coating;
Titanium porcelain;
Bond strength
- From:
Journal of Practical Stomatology
2016;32(5):635-639
- CountryChina
- Language:Chinese
-
Abstract:
Objective:To evaluate the effects of magnetron-sputtered ZrSiN/ZrO2 gradient coating on the bonding strength of commercially pure titanium to porcelain.Methods:50 cast titanium specimens were prepared according to the ISO 9693 standard,and divided into 2 groups(n =25).The ZrSiN/ZrO2 gradient coating was deposited on specimens by magnetron sputtering technique,and subsequently a low-fusing porcelain was applied for the samples in the expermental group,the samples in the control group were treated by surface sandblasting.The roughness and surface energy of the samples were measured(n =10).The bonding strength of titanium-porcelain specimens was analyzed by three-point bending test (n =10).Scanning electron microscopy (SEM) and energy-dispersive X-ray analysis (EDS) were employed to examine the properties of the delaminated and cross-sectioned surfaces.The results were analyzed by paired t-test (α =0.05) with SPSS 1 1.0 software.Results:The roughness of the experimantal group was lower(P ＜ 0.05) and the contact angle was larger(P ＜ 0.05) than those in the control group.The titanium-porcelain bond strength of gradient-coated group was greater than that of control group(P ＜0.05).The SEM and EDS examination results of delaminated and cross-sectioned surfaces also indicated that the gradient-coated group showed more porcelain residues.Conclusion:The bonding strength of porcelain-fused-to-titanium can be improved by magnetron sputtered ZrSiN/ZrO2 gradient coating.
