Studies of Quality Control of Shiwei Shujin Huoluo Powder

VernacularTitle:十味舒筋活络散质量控制研究
Author: Manqin YANG ; Ruonan XIE ; Yi CAO ; Yuewei XU ; Li WANG
Publication Type:Journal Article
Keywords: Shiwei Shujin Huoluo Powder; Emodin/analysis; Chromatography,thin layer; Chromatography,high performance liquid
From: Journal of Guangzhou University of Traditional Chinese Medicine 2014;(5):804-806,851
CountryChina
Language:Chinese
Abstract: Objective To set up the quality standard of Shiwei Shujin Huoluo Powder. Methods Rhizoma Polygoni cuspidati and Cortex Cinnamomi, the main ingredients of the powder, were identified by thin layer chromatography ( TLC) , and the content of emodin in the powder was detected by high performance liquid chromatography (HPLC) . Results The spots showed by TLC were clear without interference of the negative control. HPLC results showed that linear range of emodin was 9.30 ~ 46.52 μg·mL-1, the recovery of emodin was 96.22%, and RSD was 1.76% ( N=6) . Conclusion The established method is reliable and accurate, and can be used for quality control of Shiwei Shujin Huoluo Powder.