Limit Test for Camphor in Shujin Huoxue Pills
10.3870/yydb.2015.07.029
- VernacularTitle:舒筋活血丸中樟脑限量检查
- Author:
Zhengfeng ZHANG
;
Jia WU
;
Jing XIE
- Publication Type:Journal Article
- Keywords:
Shujin Huoxue Pills;
Camphor;
Chromatography,gas;
Quality control
- From:
Herald of Medicine
2015;(7):950-951,952
- CountryChina
- Language:Chinese
-
Abstract:
Objective To establish a method for limit test of camphor in Shujin Huoxue pills. Methods A DB-WAX (30 m×0. 32 mm,0. 25 μm) capillary column was used with a programmed temperature. Results The linear range of camphor was 1. 05-210. 00 μg·mL-1(r=1. 0). The average recovery was 101. 7%(n=9, RSD=1. 2%). Conclusion The proposed method is simple, sensitive, accurate and reproducible, which is suitable for quality control of Shujin Huoxue Pills.
