GC determination of camphor and eucalyptol in Shidi Water
- VernacularTitle:气相色谱法测定十滴水中樟脑和桉油精含量的研究
- Author:
Hua LI
;
Guohong ZHANG
;
Shoujun JIANG
;
Yan ZHONG
- Publication Type:Journal Article
- Keywords:
Shidi Water;
camphor;
eucalyptol;
GC
- From:
Chinese Traditional Patent Medicine
1992;0(07):-
- CountryChina
- Language:Chinese
-
Abstract:
AIM: To establish a method for determing camphor and eucalyptol in Shidi Water(Camphor,Rhizoma Zingiberis,Fructus Foeniculi,Cortex). METHODS: The chromatographic condition,DB-WAX capillary column(30 m?0.53 mm,1 ?m).The column temperature programming was from 65 ?C to 155 ?C(at rate of 6 ?C/min).FID Detection.The temperatrue was at 230 ?C. RESULTS: The linear range of camphor was within 0.18 mg/mL-5.78 mg/mL(r=1.000 0,n=6).The average recovery was 98.05%,RSD=0.94%.The linear range of eucalyptol was within 0.06 mg/mL-1.92 mg/ml(r=(0.999 7),n=6).The average recovery was 98.99%,RSD=1.31%. CONCLUSION: This method can be used for quality control of Shidi Water