GC/MS fingerprint of Jingu Tongxiao Pills
- VernacularTitle:筋骨痛消丸的GC/MS指纹图谱研究
- Author:
Hualing XIA
;
Xinjie ZHAO
;
Xuefeng SONG
- Publication Type:Journal Article
- Keywords:
Jingu Tongxiao Pills;
GC/MS;
fingerprint;
quality control
- From:
Chinese Traditional Patent Medicine
1992;0(12):-
- CountryChina
- Language:Chinese
-
Abstract:
AIM:To establish a GC/MS method for determining the fingerprint of Jingu Tongxiao Pills.METHODS:GC/MS condition was comprised of column:DB-1(0.25 mm?30 m,0.25 ?m);injector temperature of 250 ?C;interface temperature of 250 ?C;column temperature of 70?C(1min)4?C/min→130?C(15min)1?C/min→150?C10?C/min→250?C(7min);carrier gas:He;column pressure:60 kPa;ionization souse:EI;detector volts:1.00 kV;mass range:41～350 aum.RESULTS:17 peaks existed on the GC/MS fingerprint of Jingu Tongxiao Pills.CONCLUSION:The method can provide more information for the quality control of Jingu Tongxiao Pills.
