Fingerprints of Acanthopanax Senticosus(Puper.et Maxim) Harms by microemulsion electrokinetic chromatography
- VernacularTitle:刺五加的微乳液毛细管电动色谱指纹图谱研究
- Author:
Ran TAO
- Publication Type:Journal Article
- Keywords:
Acanthopanax Senticosus(Puper.et Maxim) Harms;
microemulsion electrokinetic capillary chromatography;
fingerprints
- From:
Chinese Traditional Patent Medicine
1992;0(01):-
- CountryChina
- Language:Chinese
-
Abstract:
AIM: The fingerprints of Acanthopanax Senticosus(Puper.et Maxim) Harms was studied by microemulsion electrokinetic chromatography(MEEKC) in comparison with micellar electrokinetic capillary chromatography(MEKC) and capillary zone electrophoresis(CZE). METHODS: The electrophoretic electrolyte was composed of a 1.0 %(w/w) SDS,6.6 %(w/w) n-butanol,0.7 %(w/w) n-heptane,91.6 %(w/w) 25 mmol/L borate solution(adjusted pH 9.5 with NaOH solution). RESULTS: The MEEKC-FP had good precision,stability and reproducibility with the relative standard deviations(RSD) of the relative migration time less than 3.4 % and the RSD of the relative peak area was about 6.3 %. CONCLUSION: This method provides a standard for the better quality controlling of Acanthopanax Senticosus(Puper.et Maxim) Harms.than MEKC and CZE.
