Identification of senkyunolide I in Guanxinning Injection chromatographic fingerprint by GC-MS and HPLC-PDA-MS-MS
- VernacularTitle:冠心宁注射液中洋川芎内酯Ⅰ的快速鉴定
- Author:
Zhangzhao JIN
;
Zhimin XIANG
;
Ming ZHU
;
Wenjun WU
;
Qing GONG
;
Ming LU
- Publication Type:Journal Article
- Keywords:
Guanxinning Injection;
chromatographic fingerprint;
preparative HPLC;
GC-MS;
senkyunolide I
- From:
Chinese Traditional Patent Medicine
1992;0(01):-
- CountryChina
- Language:Chinese
-
Abstract:
AIM: To identify an unknown peak in Guanxinning Injection(Radix et Rhizome Salviae Miltiorrhizae,Rhizoma Chuanxiong) chromatographic fingerprint. METHODS: The elution(44-46 min) separated and collected by HPLC was analyzed by GC-MS and HPLC-PDA-MS-MS. RESULTS: The unknown peak was corresponding to senkyunolidel I. CONCLUSION: It is quick method to identify the reported chemical in herbal medicine based on a small quantity of sample by GC-MS and HPLC-PDA-MS-MS.
