Extraction and seperation of indirubin in Folium Isatidis
- VernacularTitle:大青叶中靛玉红的提取分离工艺研究
- Author:
Guoxiang XIE
;
Liguo ZHANG
;
Mingfeng QIU
;
Wei JIA
- Publication Type:Journal Article
- Keywords:
Folium Isatidis;
indirubin;
column chromatograph;
NIR
- From:
Chinese Traditional Patent Medicine
1992;0(06):-
- CountryChina
- Language:Chinese
-
Abstract:
AIM: To study the suitable conditions of the extraction-separation process of the indirubin in Folium Isatidis with NIR. METHODS: The indirubin was chromatographed on an aluminium oxide column and chloroform-ethyl acetate as eluting agent,eluate was recrystalized by methanol-acetone. RESULTS: The indirubin extracted by this method was of high purity (97.78%).The sample purity was similar to reference substance one((98.01%)).The spectra of NMR and IR are the same. CONCLUSION: This method is proved to be fast,safe,lower cost,simple and has good results.
