Determination of baicalin and hesperidin in Muxiangliqi Pills by HPLC
- VernacularTitle:HPLC测定木香理气丸中黄芩苷和橙皮苷含量
- Author:
Ying YU
- Publication Type:Journal Article
- Keywords:
Muxiangliqi Pills;
baicalin;
hesperidin;
HPLC
- From:
Chinese Traditional Patent Medicine
1992;0(10):-
- CountryChina
- Language:Chinese
-
Abstract:
AIM: To establish the determination of baicalin and hesperidin in Muxiangliqi Pills (Radix Saussureae seu Vladimiriae, Pericarpium Citri Reticulatae Viride, Pericarpium Citri Reticulatae, Rhizoma Cyperi, etc.). METHODS: The determination was carried out by HPLC with octodelyl silicohydrides silanes bonded silica gel as a packing material, methanol water glacial acetic acid (35∶61∶4) as a mobile phase, detection wavelength at 283nm, flow rate at 1mL?min -1 . RESULTS: Hesperidin showed a good linear relationship at the range of 0.072?g ～0.360?g. Baicalin showed a good linear relationship at the range of 0.104?g～0.520?g. The average recoveries were 97.0% and 97.8%, respectively. RSD were 1.93% and 1.69%, respectively. CONCLUSION: The method is sensitive, accurate, reproducible, specific and can be used for quality control of Muxiangliqi Pills.
