Determination of narigin and hesperidin in Juhong Pills by HPLC
- VernacularTitle:HPLC测定橘红丸中柚皮苷、橙皮苷的含量
- Author:
Guilan DING
;
Yaguang XUE
;
Chunlai XING
;
Yingj LIU
- Publication Type:Journal Article
- Keywords:
HPLC;
Juhong Pills;
narigin;
hesperidin
- From:
Chinese Traditional Patent Medicine
1992;0(09):-
- CountryChina
- Language:Chinese
-
Abstract:
AIM: To establish the determination of narigin and hesperidin in Juhong Pills(Exocarpium, Citri Grandis, Pericarpium Citri Reticulatae, Radix Angelicae Sinensis, etc.). METHODS: The extraction was completed with ether. The Shim-pack ODS(?6.0mm?150mm) column was used with mobile phase of CH 3OH-CH 3COOH-H 2O(30∶4∶60). The detection wavelength was at 283nm. RESULTS: The linear range for narigin was 0.072～1.43?g, r=0.9999 and the linear range for hesperidin was 0.068～1.37?g, r=0.9999, respectively. Both the average recoveries were 99.3% and 99.4%, respectively. Both RSD were 0.6%(n=5). CONCLUSION: The method is simple and the result is reliable.
