Determination of imperatorin in Qianzhi Capsules by RP-HPLC
- VernacularTitle:RP-HPLC测定茜芷胶囊中欧前胡素的含量
- Author:
Xueju ZHANG
;
Wenbo SU
;
Xuefang YIN
;
Ying YE
- Publication Type:Journal Article
- Keywords:
Qianzhi Capsules;
imperatorin;
RP-HPLC
- From:
Chinese Traditional Patent Medicine
1992;0(09):-
- CountryChina
- Language:Chinese
-
Abstract:
AIM:To determine imperatorin in Qianzhi Capsules(Radix Rubiae, Radix Angelicae Dahuricae, etc.). METHODS:RP-HPLC was applied. The mobile phase consisted of methanol: 5% phosphoric acid solution(70∶30). The detection wavelength was at 248nm and the flow rate was 1.0mL?min -1. RESULTS:The linearity was obtained in the range of 12~60?g?mL -1(r=0.9998). The average recovery was 99.8% with relative standard deviation of 1.0%. CONCLUSION:The method was simple and reliable.