A new calibration-free quantitative method for near-infrared spectroscopy
- VernacularTitle:一种无校正集的近红外光谱定量分析的新方法：相似区间最小值法
- Author:
Xueyi ZHU
- Publication Type:Journal Article
- Keywords:
near-infrared spectroscopy;
quantitative analysis;
calibration-free method
- From:
Academic Journal of Second Military Medical University
1985;0(06):-
- CountryChina
- Language:Chinese
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Abstract:
Objective:To develop a new quantitative method without calibration set for near-infrared spectroscopy(NIR). Methods:The new calibration-free NIR method was based on a spectrum of the sample and a spectrum of the mixture.The similar intervals between the spectra of the sample and the mixture were obtained through second derivation,differential spectra and calculation of similarity.Then statistical quantitative analysis was performed.Results:The contents of 3 components in 3 samples were determined with the new method;the average recovery was 100.9% and the relative standard deviation was 6.1% (n=9).Conclusion:Satisfactory results can be obtained by this new method without traditional calibration set.The new method provides an alternative for the quantitative analysis in NIRs and has a promising future.
