Determination of Tin in Air by Microwave Digestion-HG-AFS
- VernacularTitle:作业场所空气中锡的微波消解-氢化物发生原子荧光光度测定法
- Author:
Feirong ZHAO
;
Qian PENG
;
Yiwen CHEN
- Publication Type:Journal Article
- Keywords:
Spectrophotometry;
Air pollution;
Tin;
Atomic fluorescence spectrometry;
Microwave digestion
- From:
Journal of Environment and Health
1989;0(06):-
- CountryChina
- Language:Chinese
-
Abstract:
Objective To develop a method for determination of tin in the air of workplace by microwave digestion-HG-AFS. Methods The air samples were collected and the concentration of tin was determined by microwave digestion-HG-AFS and the parameters of atomic fluorescence spectrometry were studied. Results In the optimum condition, the detection limit of tin was 0.3 ?g /L, the lowest detected concentration of tin in the samples was 0.000 1 mg/m3 (based on 75 L air sample), the RSD was 2.7%-3.5%, the rate of recovery was in the range of 96.5%-104.7%. Conclusion The method is rapid, convenient, accurate, sensitive and suitable for determination of tin in the air of workplace.