Study on Preparation and Quality Standard of Kuijieyu Enemas
- VernacularTitle:溃结愈灌肠剂的制备及质量标准研究
- Author:
Xinguang ZHANG
;
Dongmei WANG
;
Shaobo DING
- Publication Type:Journal Article
- Keywords:
Kuijieyu enemas;
Preparation;
Quality standard;
Baicalin;
TLC;
HPLC
- From:
China Pharmacy
2005;0(23):-
- CountryChina
- Language:Chinese
-
Abstract:
OBJECTIVE: To prepare Kuijieyu enemas and establish its quality standard.METHODS: Most of traditional Chinese medicines in prescription were decocted using water and some were crushed.Then they were concentrated to prepare enemas.Pueraria lobata,Rhizoma Coptidis,Scutellaria baicalensis in Kuijieyu enemas were qualitatively identified by TLC.The content of baicalin in Kuijieyu enemas was determined by HPLC.RESULTS: The TLC spots were clear,well-separated and specific.The linear range of baicalin were 210~1 750 ?g(r=0.999 9) with an average recovery of 99.13% (RSD=1.1%,n=6).CONCLUSION: The preparation process is simple and convenient.The quality control method is simple,reliable,specific and reproducible.