Quality Criteria of Lianqi Bushen Capsule
- VernacularTitle:莲杞补肾胶囊质量标准研究
- Author:
Jiwei XIA
;
Youcai WAN
;
Yun LI
;
Daoqing LIU
- Publication Type:Journal Article
- Keywords:
Lianqi bushen capsule;
Quality creteria;
Panax ginseng;
Trigonelline;
TLC;
RP-HPLC
- From:
China Pharmacy
2001;0(07):-
- CountryChina
- Language:Chinese
-
Abstract:
OBJECTIVE:To establish the quality standard of Lianqi bushen capsule.METHODS: TLC was employed to identify Panax ginseng in Lianqi bushen capsule,while the content of trigonelline was determined by RP-HPLC.The determination was performed on Kromasil C18(150 mm?4.6 mm,5 ?m)column and mobile phase consisted of methanol-0.05%sodium dodecyl sulfonate-acetic acid(20 ∶ 80 ∶ 0.1)with flow rate of 1 mL?min-1.The detection wavelength was set at 265 nm and column temperature was set at 30 ℃.RESULTS:P.ginseng can be identified by TLC.The linear range of trigonelline was 10~200 ?g?mL-1(r=0.999 9) and average recovery was 98.86%(RSD=1.4%,n=5).CONCLUSION:The standard is used for the quality control of Lianqi bushen capsule.