Content Determination of Paeoniflorin in Shaofuzhuyu Superfine Powders Granules by HPLC
- VernacularTitle:反相高效液相色谱法测定少腹逐淤微粉颗粒中芍药苷的含量
- Author:
Xin HUANG
;
Lequn SU
;
Yudong HAN
;
Fengqin LIU
- Publication Type:Journal Article
- Keywords:
HPLC;
Shaofuzhuyu superfine powder granules;
Paeoniflorin;
Content
- From:
China Pharmacy
1991;0(06):-
- CountryChina
- Language:Chinese
-
Abstract:
OBJECTIVE:To determine content of paeoniflorin in shaofuzhuyu superfine powder granules by HPLC. METHODS: The separation was performed on C18 chromatographic column, the mobile phase was methanol -0.05mol/L KH2PO4(40∶65)with a flow speed at 1ml/min, detection wavelength at 230nm and column temperature at 30℃. RESULTS:The linear range of paeoniflorin was 15.04～752.00?g/ml(r=0.9 998,n=6),the mean recovery rate was 103.3%(RSD=1.53%,n=3).CONCLUSION:This method was simple, accurate, good in recurrence and high in precision, and which can be used for the contents determination and the quality control of the shaofuzhuyu superfine powder granules.
