Detection of aconitine in biological samples by GC/MS
- VernacularTitle:生物检材中乌头碱的GC/MS分析
- Author:
Zhaohong WANG
;
Yi HE
;
Jizong ZHANG
- Publication Type:Journal Article
- Keywords:
Forensic toxicological analysis;
biological tissues;
Aconitine;
GC/MS
- From:
Chinese Journal of Forensic Medicine
1987;0(03):-
- CountryChina
- Language:Chinese
-
Abstract:
Objective To establish a method used for qualitative determination of aconitine in biological samples by GC/MS. Methods using MSTFA as derivative reagent and pyridine as solvent leaving in 60℃ for 30min then detected by GC/MS-SIM. Results The limit of detection of aconitine was 20ng (S/N≥100). Conclusion This method is sensitive, fast, and accurate. It is useful for forensic medical practice.
