Chemical constituents from the rhizomas of Smilax glauco-china
10.3969/j.issn.1001-1528.2017.03.020
- VernacularTitle:黑果菝葜根茎化学成分的研究
- Author:
Min LIU
;
Xiaohua ZHENG
;
Genhua ZHU
;
Huilian HUANG
;
Jicheng SHU
;
Feng SHAO
;
Ronghua LIU
- Keywords:
Smilax glauco-china Warb;
rhizomas;
chemical constituents;
isolation and identification
- From:
Chinese Traditional Patent Medicine
2017;39(3):540-543
- CountryChina
- Language:Chinese
-
Abstract:
AIM To study the chemical constituents from the rhizomas of Smilax glauco-china Warb.METHODS The n-butanol fraction of ethanol extract of S.glauco-china was isolated and purified by silica,Sephadex LH-20 and semi-preparative column,then the structures of obtained compounds were identified by physicochemical properties and spectral data.RESULTS Ten compounds were isolated and identified as phenethanol-β-D-gentiobioside (1),2-phenylethyl-O-β-D-xylopyranosyl-(1 →6)-β-D-glucopyranoside (2),phenylethyl D-rutinoside (3),phenylethyl β-D-glucoside (4),hydrangeifolin Ⅰ (5),icariside D1 (6),calophymembranside B (7),2-hydroxyphenol-1-O-β-D-glucopyranosyl-(6 → 1)-α-L-rhamnopyranoside (8),β-sitosterol (9),daucosterol (10).CONCLUSION All the compounds are isolated from this plant for the first time.
