Qualitative Detection of Donkey-hide Gelatin in Fufang Ejiao Buxue Granule by UPLC-QQQ/MS
- VernacularTitle:超高效液相色谱-三重四极杆质谱法检测复方阿胶补血颗粒中的阿胶
- Author:
Hongyu CHEN
;
Jinping LI
;
Wenli LI
;
Qing YANG
;
Da TONG
;
Jieying GAO
;
Xiaoyan HUANG
- Publication Type:Journal Article
- Keywords:
UPLC/QQQ-MS;
Fufang Ejiao Buxue granule;
Donkey-hide gelatin;
Characteristic molecular ion peak
- From:
China Pharmacist
2016;19(6):1052-1054
- CountryChina
- Language:Chinese
-
Abstract:
Objective:To establish an analytical method for the identification of donkey-hide gelatin in Fufang Ejiao Buxue gran-ule.Methods:The identification of donkey-hide gelatin in Fufang Ejiao Buxue granule was established by rapid resolution liquid chro -matography (UPLC) coupled with triple quadruple mass spectrometry (QQQ-MS).Results: The characteristic molecular peaks of donkey-hide gelatin were detected in ten batches of commercial samples .Conclusion:The present method is specific , precise and reli-able, and suitable for the identification of donkey-hide gelatin in Fufang Ejiao Buxue granule .The method provides scientific reference for the study of quality control method for gelatin ingredients in Chinese patent medicines .
