Quality Standard of Shenbo Fuyanning Suppository
10.3870/j.issn.1004-0781.2015.12.025
- VernacularTitle:参柏妇炎宁栓质量标准
- Author:
Songqiao FENG
;
Yiqin FEI
- Publication Type:Journal Article
- Keywords:
Shenbo Fuyanning suppositories;
Berberine;
hydrochlorid;
Chromatography;
thin layer;
Chromatography;
high performance liquid
- From:
Herald of Medicine
2015;34(12):1649-1652
- CountryChina
- Language:Chinese
-
Abstract:
Objective To establish a method for quality control of Shenbo Fuyanning suppositories. Methods Sophorae flavescentis Radix, Rhizoma dioscoreae Hypoglaucae, and Cnidii fructus were identified by thin layer chromatography ( TLC) , and the content of berberine hydrochloride was determined by HPLC. Results The TLC spots were clear and the negative control had no interference.Berberine hydrochloride had a linear relationship in the range of 0.079-0.790 μg, and the average recovery was 99.3%(RSD=0.70%,n=6). Conclusion The method is accurate, reliable and feasible, and can be used in the quality control of the Shenbo Fuyanning suppository effectively.
