Determination of Phenoxyacetic Acid and 2,4-Dichlorophenoxyacetic Acid Using Solid-phase Extraction and High Performance Liquid Chromatography
- VernacularTitle:固相萃取富集高效液相色谱法测定苯氧乙酸和2,4-二氯苯氧乙酸
- Author:
Jinchang LI
;
Lu WANG
;
Mingyou HAN
;
Ming BAO
;
Guang WANG
;
Yuanhong WANG
- Publication Type:Journal Article
- From:
Chinese Journal of Analytical Chemistry
2001;29(5):580-582
- CountryChina
- Language:Chinese
-
Abstract:
A high performance liquid chromatographic method for the determination of phenoxyacetic acid and 2,4-dichlorophroxyacetic acid in environnmental waters was described.Phenoxyacetic acid and 2, 4-dichioropheroxyacetic acid in sample were enriched on Sep-Pak C18 column,and methanol was employed as elutent.The shim-pack CLC ODS (150mm×6.0mm i.d.) column was used as separation column at 40°C and eluted with methanol-water (9:1,V/V)(pH 3.0) at flow rate of 1.0mL/min,the detection wavelength was 275 nm.The recoveries of the two compounds were＞98%.The detection limit was 0.04mg/L.
