Study on quality standard of extracts from Rhizoma Zingiberis by supercritical fluid extraction.
- Author:
Qing MENG
1
;
Yi-fan FENG
;
Xiao-ling GUO
;
Geng-fu CHEN
;
Jian-cong CAI
Author Information
- Publication Type:Journal Article
- MeSH: Catechols; Chromatography, Supercritical Fluid; methods; Drugs, Chinese Herbal; chemistry; isolation & purification; Fatty Alcohols; analysis; Ginger; chemistry; Phenols; analysis; Plants, Medicinal; chemistry; Quality Control; Rhizome; chemistry
- From: China Journal of Chinese Materia Medica 2005;30(10):750-752
- CountryChina
- Language:Chinese
-
Abstract:
OBJECTIVETo establish the quality standard of extracts from Rhizoma Zingiberis by supercritical CO2 fluid extraction.
METHODThe extracts were identified by TLC. The total phenols and the 6-gingerol were determined by dual-wavelength UV spectrophotometry and HPLC separately.
RESULTThe recovery of total phenols was 97.7% (RSD 2.0%). The linear range of 6-gingerol is 0.20-2.0 microg, the average recovery was 97.7% (RSD 2.0%).
CONCLUSIONThe method is convenient for a good resolution and can be used for the quality control of extracts from Rhizoma Zingiberis.