Chemical constituents in higher polar substances from Desmodium caudatum.
- Author:
Dan ZHU
;
Di WANG
;
Guang-Hui WANG
;
Zhi-Jian GUO
;
Xiu-Hong ZOU
;
Ting LIN
;
Hai-Feng CHEN
- Publication Type:Journal Article
- MeSH:
Apigenin;
chemistry;
isolation & purification;
Drugs, Chinese Herbal;
chemistry;
isolation & purification;
Fabaceae;
chemistry;
Molecular Structure;
Saponins;
chemistry;
isolation & purification;
Spectrometry, Mass, Electrospray Ionization
- From:
China Journal of Chinese Materia Medica
2014;39(16):3112-3116
- CountryChina
- Language:Chinese
-
Abstract:
In this study the chemical constituents of the higher polar sustances from Desmodium caudatum were investigated.The compounds were isolated by using column chromatographies over silicagel, polyamide, ODS, Sephadex LH-20, and preparative HPLC. The structures of these compounds were identified on the basis of NMR and MS spectra. Thirteen compounds were obtained and their structures were identified as vanillin(1), loliolide(2), indole-3-carboxaldehyde(3), salicylic acid(4), swertisin(5), saccharumoside C(6), isosinensin (7), kaempferol 3-O-β-D-glucopyranoside-7-O-α-L-rhamnopyranoside (8), isovitexin (9), vitexin (10), nothofagin(11), resveratroloside (12), and 2"-α-rhamnopyranosyl-7-O-methylvitexin (13). Except for compound 5, the remaining compounds were isolated from D. caudatum for the first time. Compounds 2, 3, 6-8, 11-13 were separated from the genus Desmodium for the first time.