HPLC-ESI-MS(n) analysis of chemical constituents in Semen Ziziphi Spinosae.
- Author:
Weiji WANG
1
;
Jianguang LUO
;
Lingyi KONG
Author Information
- Publication Type:Journal Article
- MeSH: Chromatography, High Pressure Liquid; methods; Drugs, Chinese Herbal; chemistry; Flavonoids; chemistry; Saponins; chemistry; Semen; chemistry; Spectrometry, Mass, Electrospray Ionization; methods
- From: China Journal of Chinese Materia Medica 2009;34(21):2768-2773
- CountryChina
- Language:Chinese
-
Abstract:
OBJECTIVETo study on the chemical constituents of effective part of Semen Ziziphi Spinosae.
METHODThe sample was extracted with methanol and purified by macroporous resin. The structures were identified by high performance liquid chromatography/electrospray ionization with multi-stage tandem mass spectrometry.
RESULTThirteen compounds were identified from the effective part of Semen Ziziphi Spinosae.
CONCLUSIONThe method is simple and rapid for the identification of the flavonoids and triterpenoid saponins from Semen Ziziphi Spinosae.
