RP-HPLC characteristics of dragon's blood.
- Author:
Xiu-Li GAO
1
;
Qian JIANG
;
Peng-Jiao WANG
;
Min ZHANG
Author Information
- Publication Type:Journal Article
- MeSH: Chromatography, High Pressure Liquid; methods; Dracaena; chemistry; Plant Extracts; analysis; isolation & purification; standards; Plants, Medicinal; chemistry; Quality Control; Reproducibility of Results; Resins, Plant; analysis; isolation & purification; standards
- From: China Journal of Chinese Materia Medica 2007;32(19):2025-2027
- CountryChina
- Language:Chinese
-
Abstract:
OBJECTIVETo study the fingerprint of dragon's blood resina draconis by high performance liquid chromatography.
METHODThe samples are extracted with methanol and separated on a Eclipse XDB-C18 column (4.6 mm x 150 mm, 5 microm) with the mobile phase of acetonitrile-H2O in gradient mode, and the flow rate was 1.0 mL x min(-1), the detection wavelength was 275 nm and the temperature of column was 40 degrees C. Loureirin B was used as the reference compound.
RESULTHPLC fingerprint of dragon's blood was established and the similarity of the fingerprint was compared.
CONCLUSIONThe method is simple, accurate, and can be used to control the quality of dragon's blood.
