HPLC fingerprint of glycyrrhizea radix et rhizoma praeparata cum melle.
- Author:
Lei SUN
;
Yong JIN
;
Xiao-Qing LIU
;
Shan-Yi QIAO
;
Song GAO
;
Yan-Zhong CHE
- Publication Type:Journal Article
- MeSH:
China;
Chromatography, High Pressure Liquid;
methods;
Drugs, Chinese Herbal;
chemistry;
Glycyrrhiza uralensis;
chemistry;
Mass Spectrometry;
Quality Control;
Rhizome;
chemistry
- From:
China Journal of Chinese Materia Medica
2014;39(11):2056-2059
- CountryChina
- Language:Chinese
-
Abstract:
The chromatographic fingerprint was established by eluting with the mobile phase consisted of acetonitrile and 0.2% formic acid water on an Agilent TC-C18 (2) column (4.6 mm x 250 mm, 5 microm). Six chromatographic peaks were identified by HPLC-MS/MS method. Ten batches of Glycyrrhizea Radix et Rhizoma Praeparata Cum Melle were determined, and the similarity was arranged from 0.72 to 0.99. Good precision, stability and repeatability were obtained, and this study provides a reference for the quality control of Glycyrrhizea Radix et Rhizoma Praeparata Cum Melle.
