Studies on chemical constituents and volatile oil of Xiaochengqi decoction.
- Author:
Miao-Xuan FAN
1
;
Hong-Jie WANG
;
Xiao-Ming LI
;
Peng-Yue LI
;
Bao-Lin BIAN
Author Information
- Publication Type:Journal Article
- MeSH: Anthraquinones; chemistry; Biphenyl Compounds; chemistry; Cinnamates; chemistry; Cyclohexenes; chemistry; Drugs, Chinese Herbal; chemistry; Emodin; analogs & derivatives; chemistry; Gallic Acid; chemistry; Gas Chromatography-Mass Spectrometry; Lignans; chemistry; Monoterpenes; chemistry; Oils, Volatile; chemistry; Sitosterols; chemistry; Terpenes; chemistry
- From: China Journal of Chinese Materia Medica 2008;33(9):1027-1031
- CountryChina
- Language:Chinese
-
Abstract:
OBJECTIVETo study the chemical constituents and volatile oil of Xiaochengqi decoction.
METHODThe constituents in decoction were separated by means of column chromatography and their structures were identified by spectral data and compared with literature data. As well as the volatile oil of Xiaochengqi Fang were analyzed and identified by GC-MS.
RESULTEleven compounds were isolated and identified as chrysophanol (1), physcion (2), magnolol (3), beta-sitosterol (4), sitosterol trans-cinnamic acid (5), emodin (6), aloe emodin (7), rhein (8), gallic acid (9), chrysophanol-8-O-beta-D-glucopyranoside (10), aurantiamarin (11). The volatile oils extracted with steam distillation from Xiaochengqi were identified 67 components, and the main components are including.
CONCLUSIONAll of the eleven compounds were isolated from Xiaochengqi decoction for the first time and the study on their activities in Chinese prescription is being carried out. D-limonene (42.61%), p-cymene (16.43%), and 8-terpinene (14.46%).