Study on active components alignment of alkaloids in extractive of Folium aconiti kusnezoffii by ESI-MS.
- Author:
Ya TU
1
;
Gui-Jun ZHANG
;
Shu-Min WANG
;
Zhi-Qiang LIU
Author Information
- Publication Type:Journal Article
- MeSH: Aconitum; chemistry; Alkaloids; analysis; isolation & purification; Drugs, Chinese Herbal; chemistry; Spectrometry, Mass, Electrospray Ionization
- From: China Journal of Chinese Materia Medica 2008;33(7):789-790
- CountryChina
- Language:Chinese
-
Abstract:
OBJECTIVETo analyze the active components alignment of aconitum alkaloids on extractive of Folium Aconiti Kusnezoffii and its decoction.
METHODThe analysis was performed by the method of ESI-MS.
RESULTThe biester-type and the triester-type diterpenoid aconitum alkaloids were hydrolysed after boiling in water, the former was hydrolyzed to 14-benzoylaconine and aconine, the latter to 3-acylaconine.
CONCLUSIONThe method is simple rapid and sensitive, provide a new instrumentality to analyze the active components alignment of aconitum alkaloids on extractive of folium aconiti kusnezoffii.